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MS 28

Base Information
  • Chemical Name:MS 28
  • CAS No.:117523-45-2
  • Molecular Formula:C24H27 N3 O2
  • Molecular Weight:389.49
  • Hs Code.:
  • Mol file:117523-45-2.mol
MS 28

Synonyms:Compound28; MS 28; OHM 3568

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Chemical Property of MS 28
Chemical Property:
  • Vapor Pressure:1.46E-12mmHg at 25°C 
  • Melting Point:198-199.5 °C 
  • Boiling Point:559.8°Cat760mmHg 
  • PKA:8.60±0.10(Predicted) 
  • Flash Point:292.3°C 
  • PSA:49.58000 
  • Density:1.176g/cm3 
  • LogP:4.27480 
Purity/Quality:
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MSDS Files:

SDS file from LookChem

Useful:
Technology Process of MS 28

There total 6 articles about MS 28 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With triethylamine; In chloroform; for 0.5h; Ambient temperature;
DOI:10.1021/jm00123a028
Guidance literature:
Multi-step reaction with 4 steps
1: 35 percent / 3-chloroperoxybenzoic acid / CHCl3 / 4 h / Heating
2: 26 percent / Na2CO3, KI / 3-methyl-butan-1-ol / 48 h / Heating
3: 61 percent / PCl3 / CHCl3 / 2 h / Heating
4: 75 percent / Et3N / CHCl3 / 0.5 h / Ambient temperature
With sodium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; potassium iodide; phosphorus trichloride; In i-Amyl alcohol; chloroform;
DOI:10.1021/jm00123a028
Guidance literature:
Multi-step reaction with 3 steps
1: 26 percent / Na2CO3, KI / 3-methyl-butan-1-ol / 48 h / Heating
2: 61 percent / PCl3 / CHCl3 / 2 h / Heating
3: 75 percent / Et3N / CHCl3 / 0.5 h / Ambient temperature
With sodium carbonate; triethylamine; potassium iodide; phosphorus trichloride; In i-Amyl alcohol; chloroform;
DOI:10.1021/jm00123a028
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