N₂-[tert-butoxycarbonyl]-N₁-[(2,3-cis)-4-oxo-2-phenyl-2,3,4,5-tetrahydro-1,5-benzothiazepin-3-yl]-L-alaninamide

Base Information

• Chemical Name: N₂-[tert-butoxycarbonyl]-N₁-[(2,3-cis)-4-oxo-2-phenyl-2,3,4,5-tetrahydro-1,5-benzothiazepin-3-yl]-L-alaninamide
• CAS No.: 680232-25-1
• Molecular Formula: C₂₃H₂₇N₃O₄S
• Molecular Weight: 441.551

Synonyms:N₂-[tert-butoxycarbonyl]-N₁-[(2,3-cis)-4-oxo-2-phenyl-2,3,4,5-tetrahydro-1,5-benzothiazepin-3-yl]-L-alaninamide

Chemical Property of N₂-[tert-butoxycarbonyl]-N₁-[(2,3-cis)-4-oxo-2-phenyl-2,3,4,5-tetrahydro-1,5-benzothiazepin-3-yl]-L-alaninamide

Chemical Property:

Purity/Quality:

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Technology Process of N₂-[tert-butoxycarbonyl]-N₁-[(2,3-cis)-4-oxo-2-phenyl-2,3,4,5-tetrahydro-1,5-benzothiazepin-3-yl]-L-alaninamide

There total 1 articles about N₂-[tert-butoxycarbonyl]-N₁-[(2,3-cis)-4-oxo-2-phenyl-2,3,4,5-tetrahydro-1,5-benzothiazepin-3-yl]-L-alaninamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2,3-cis)-3-amino-2-phenyl-2,3-dihydro-1,5-benzothiazepin-4(5H)-one hydrobromide + L-N-Boc-Ala (15761-38-3) → N2-[tert-butoxycarbonyl]-N1-[(2,3-cis)-4-oxo-2-phenyl-2,3,4,5-tetrahydro-1,5-benzothiazepin-3-yl]-L-alaninamide (680232-25-1)

Guidance literature:

With dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 20 ℃; for 16h;

Reference yield:

N2-[tert-butoxycarbonyl]-N1-[(2,3-cis)-4-oxo-2-phenyl-2,3,4,5-tetrahydro-1,5-benzothiazepin-3-yl]-L-alaninamide (680232-25-1) → N1-[(2,3-cis)-4-oxo-2-phenyl-2,3,4,5-tetrahydro-1,5-benzothiazepin-3-yl]-L-alaninamide (680232-26-2)

Guidance literature:

N₂-[tert-butoxycarbonyl]-N₁-[(2,3-cis)-4-oxo-2-phenyl-2,3,4,5-tetrahydro-1,5-benzothiazepin-3-yl]-L-alaninamide; With trifluoroacetic acid; for 0.166667h;

With potassium carbonate; In water;

upstream raw materials:

L-N-Boc-Ala

Downstream raw materials:

N₁-[(2,3-cis)-4-oxo-2-phenyl-2,3,4,5-tetrahydro-1,5-benzothiazepin-3-yl]-L-alaninamide

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