Technology Process of 4-(4-Heptyl-cyclohexyl)-benzamide
There total 11 articles about 4-(4-Heptyl-cyclohexyl)-benzamide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 2.) 10percent aq. HCl / 1.) diethyl ether, 1 h, heating
2: p-toluenesulfonic acid / toluene / Heating
3: H2 / 10percent Pd/C / ethanol
4: AlCl3 / 1,2-dichloro-ethane / 0.5 h
5: aq. NaOH, Br2 / dioxane / 3 h / 35 - 40 °C
6: SOCl2 / 1 h / Heating
7: 25percent aq. NH4OH
With
hydrogenchloride; ammonium hydroxide; sodium hydroxide; aluminium trichloride; thionyl chloride; hydrogen; bromine; toluene-4-sulfonic acid;
palladium on activated charcoal;
In
1,4-dioxane; ethanol; 1,2-dichloro-ethane; toluene;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 2.) 10percent aq. HCl / 1.) diethyl ether, 1 h, heating
2: p-toluenesulfonic acid / toluene / Heating
3: H2 / 10percent Pd/C / ethanol
4: AlCl3 / 1,2-dichloro-ethane / 0.5 h
5: aq. NaOH, Br2 / dioxane / 3 h / 35 - 40 °C
6: SOCl2 / 1 h / Heating
7: 25percent aq. NH4OH
With
hydrogenchloride; ammonium hydroxide; sodium hydroxide; aluminium trichloride; thionyl chloride; hydrogen; bromine; toluene-4-sulfonic acid;
palladium on activated charcoal;
In
1,4-dioxane; ethanol; 1,2-dichloro-ethane; toluene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: H2 / 10percent Pd/C / ethanol
2: AlCl3 / 1,2-dichloro-ethane / 0.5 h
3: aq. NaOH, Br2 / dioxane / 3 h / 35 - 40 °C
4: SOCl2 / 1 h / Heating
5: 25percent aq. NH4OH
With
ammonium hydroxide; sodium hydroxide; aluminium trichloride; thionyl chloride; hydrogen; bromine;
palladium on activated charcoal;
In
1,4-dioxane; ethanol; 1,2-dichloro-ethane;