3-deoxy-1,2-O-isopropylidene-5-O-(4-methylbenzoyl)-α-D-erythro-pentofuranose

Base Information

Chemical Name:3-deoxy-1,2-O-isopropylidene-5-O-(4-methylbenzoyl)-α-D-erythro-pentofuranose
CAS No.:161110-10-7
Molecular Formula:C₁₆H₂₀O₅
Molecular Weight:292.332
Hs Code.:

Synonyms:3-deoxy-1,2-O-isopropylidene-5-O-(4-methylbenzoyl)-α-D-erythro-pentofuranose

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Chemical Property of 3-deoxy-1,2-O-isopropylidene-5-O-(4-methylbenzoyl)-α-D-erythro-pentofuranose

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Technology Process of 3-deoxy-1,2-O-isopropylidene-5-O-(4-methylbenzoyl)-α-D-erythro-pentofuranose

There total 6 articles about 3-deoxy-1,2-O-isopropylidene-5-O-(4-methylbenzoyl)-α-D-erythro-pentofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 642085-94-7
4-Methyl-benzoic acid (3aR,5R,6S,6aR)-6-(imidazole-1-carbothioyloxy)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-ylmethyl ester

: 161110-10-7
3-deoxy-1,2-O-isopropylidene-5-O-(4-methylbenzoyl)-α-D-erythro-pentofuranose

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; for 2h; Heating;
DOI:10.1016/S0968-0896(02)00535-7

Reference yield: 72.0%

: 171603-61-5
4-Methyl-benzoic acid (3aR,5R,6S,6aR)-2,2-dimethyl-6-phenoxythiocarbonyloxy-tetrahydro-furo[2,3-d][1,3]dioxol-5-ylmethyl ester

: 161110-10-7
3-deoxy-1,2-O-isopropylidene-5-O-(4-methylbenzoyl)-α-D-erythro-pentofuranose

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 80 ℃; for 6h;
DOI:10.1080/15257779408012162

Reference yield:

: 75096-60-5
1,2-O-isopropylidene-5-O-(4-toluoyl)-D-xylofuranose

: 161110-10-7
3-deoxy-1,2-O-isopropylidene-5-O-(4-methylbenzoyl)-α-D-erythro-pentofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / 1,2-dichloro-ethane / 1.5 h / Heating

2: 100 percent / Bu₃SnH; AIBN / toluene / 2 h / Heating

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In 1,2-dichloro-ethane; toluene; 2: Barton-McCombie reaction;
DOI:10.1016/S0968-0896(02)00535-7