methyl (4'-O-hexanoylglycitein-7-yl β-D-2'',3'',4''-triacetylglucopyranosid)uronate

Base Information

Chemical Name:methyl (4'-O-hexanoylglycitein-7-yl β-D-2'',3'',4''-triacetylglucopyranosid)uronate
CAS No.:918158-56-2
Molecular Formula:C₃₅H₃₈O₁₅
Molecular Weight:698.678
Hs Code.:

Synonyms:methyl (4'-O-hexanoylglycitein-7-yl β-D-2'',3'',4''-triacetylglucopyranosid)uronate

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Chemical Property of methyl (4'-O-hexanoylglycitein-7-yl β-D-2'',3'',4''-triacetylglucopyranosid)uronate

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Technology Process of methyl (4'-O-hexanoylglycitein-7-yl β-D-2'',3'',4''-triacetylglucopyranosid)uronate

There total 5 articles about methyl (4'-O-hexanoylglycitein-7-yl β-D-2'',3'',4''-triacetylglucopyranosid)uronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 918158-53-9
4'-O-hexanoylglycitein

: 918158-52-8
C₂₂H₂₄F₃NO₁₁

: 918158-56-2
methyl (4'-O-hexanoylglycitein-7-yl β-D-2'',3'',4''-triacetylglucopyranosid)uronate

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 6h; Inert atmosphere; Molecular sieve;
DOI:10.1002/ejoc.200800803

Reference yield: 78.0%

: 918158-53-9
4'-O-hexanoylglycitein

: (2S,3S,4S,5R)-3,4,5-Triacetoxy-6-[2,2,2-trifluoro-N-(4-methoxy-phenyl)-acetimidoyloxy]-tetrahydro-pyran-2-carboxylic acid methyl ester

: 918158-56-2
methyl (4'-O-hexanoylglycitein-7-yl β-D-2'',3'',4''-triacetylglucopyranosid)uronate

Guidance literature:: With 4 A molecular sieve; boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 6h;
DOI:10.1016/j.tetlet.2006.10.034

Reference yield:

: 40957-83-3
glycitein

: 918158-56-2
methyl (4'-O-hexanoylglycitein-7-yl β-D-2'',3'',4''-triacetylglucopyranosid)uronate

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / t-BuOK / dimethylformamide / 35 °C

2: 78 percent / BF₃*EtO₂; 4 Angstroem molecular sieves / CH₂Cl₂ / 6 h / 20 °C

With 4 A molecular sieve; boron trifluoride diethyl etherate; potassium tert-butylate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2006.10.034