5-(p-Anisyl)-2,3,5,6-tetrahydro-7-phenyl-2-(o-tolyl)-4H-1,2,5-triazepin-4-on

Base Information

Chemical Name:5-(p-Anisyl)-2,3,5,6-tetrahydro-7-phenyl-2-(o-tolyl)-4H-1,2,5-triazepin-4-on
CAS No.:81964-27-4
Molecular Formula:C₂₄H₂₃N₃O₂
Molecular Weight:385.466
Hs Code.:

Synonyms:5-(p-Anisyl)-2,3,5,6-tetrahydro-7-phenyl-2-(o-tolyl)-4H-1,2,5-triazepin-4-on

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Chemical Property of 5-(p-Anisyl)-2,3,5,6-tetrahydro-7-phenyl-2-(o-tolyl)-4H-1,2,5-triazepin-4-on

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Technology Process of 5-(p-Anisyl)-2,3,5,6-tetrahydro-7-phenyl-2-(o-tolyl)-4H-1,2,5-triazepin-4-on

There total 3 articles about 5-(p-Anisyl)-2,3,5,6-tetrahydro-7-phenyl-2-(o-tolyl)-4H-1,2,5-triazepin-4-on which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 81964-24-1
syn-(E)-α-(N-Iodacetyl-p-anisidino)acetophenon-o-tolylhydrazon

: 81964-27-4
5-(p-Anisyl)-2,3,5,6-tetrahydro-7-phenyl-2-(o-tolyl)-4H-1,2,5-triazepin-4-on

Guidance literature:: With sodium hydroxide; Aliquat 336; In benzene; for 8h;

Reference yield:

: 81964-21-8
syn-(E)-α-(N-Chloracetyl-p-anisidino)acetophenon-o-tolylhydrazon

: 81964-27-4
5-(p-Anisyl)-2,3,5,6-tetrahydro-7-phenyl-2-(o-tolyl)-4H-1,2,5-triazepin-4-on

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / NaI / acetone / 0.5 h / Heating

2: 76 percent / 1N NaOH, tricaprylmethylammonium chloride / benzene / 8 h

With sodium hydroxide; Aliquat 336; sodium iodide; In acetone; benzene;

Reference yield:

: 69604-55-3
(4-Methoxy-phenyl)-[2-phenyl-2-(o-tolyl-hydrazono)-ethyl]-amine

: 81964-27-4
5-(p-Anisyl)-2,3,5,6-tetrahydro-7-phenyl-2-(o-tolyl)-4H-1,2,5-triazepin-4-on

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / sodium acetate, water / acetic acid / 0.5 h

2: 92 percent / NaI / acetone / 0.5 h / Heating

3: 76 percent / 1N NaOH, tricaprylmethylammonium chloride / benzene / 8 h

With sodium hydroxide; water; sodium acetate; Aliquat 336; sodium iodide; In acetic acid; acetone; benzene;