ethyl {[2-methyl-4-({3-[3-methyl-6-(trifluoromethyl)-1-benzothien-2-yl]heptyl}oxy)phenyl]oxy}acetate

Base Information

• Chemical Name: ethyl {[2-methyl-4-({3-[3-methyl-6-(trifluoromethyl)-1-benzothien-2-yl]heptyl}oxy)phenyl]oxy}acetate
• CAS No.: 863119-25-9
• Molecular Formula: C₂₈H₃₃F₃O₄S
• Molecular Weight: 522.629

Synonyms:ethyl {[2-methyl-4-({3-[3-methyl-6-(trifluoromethyl)-1-benzothien-2-yl]heptyl}oxy)phenyl]oxy}acetate

Chemical Property of ethyl {[2-methyl-4-({3-[3-methyl-6-(trifluoromethyl)-1-benzothien-2-yl]heptyl}oxy)phenyl]oxy}acetate

Chemical Property:

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Technology Process of ethyl {[2-methyl-4-({3-[3-methyl-6-(trifluoromethyl)-1-benzothien-2-yl]heptyl}oxy)phenyl]oxy}acetate

There total 1 articles about ethyl {[2-methyl-4-({3-[3-methyl-6-(trifluoromethyl)-1-benzothien-2-yl]heptyl}oxy)phenyl]oxy}acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(4-hydroxy-2-methylphenoxy)acetic acid ethyl ester (403612-14-6) + 2-[1-(2-bromoethyl)pentyl]-3-methyl-6-(trifluoromethyl)-1-benzothiophene (863119-18-0) → ethyl {[2-methyl-4-({3-[3-methyl-6-(trifluoromethyl)-1-benzothien-2-yl]heptyl}oxy)phenyl]oxy}acetate (863119-25-9)

Guidance literature:

With caesium carbonate; In acetonitrile; at 20 ℃; for 120h;

Reference yield:

ethyl {[2-methyl-4-({3-[3-methyl-6-(trifluoromethyl)-1-benzothien-2-yl]heptyl}oxy)phenyl]oxy}acetate (863119-25-9) → {[2-methyl-4-({3-[3-methyl-6-(trifluoromethyl)-1-benzothien-2-yl]heptyl}oxy)phenyl]oxy}acetic acid

Guidance literature:

With methanol; sodium hydroxide; water; In tetrahydrofuran; at 20 ℃; for 1h;

Reference yield:

ethyl {[2-methyl-4-({3-[3-methyl-6-(trifluoromethyl)-1-benzothien-2-yl]heptyl}oxy)phenyl]oxy}acetate (863119-25-9) → ethyl {[2-methyl-4-({(3R)-3-[3-methyl-6-(trifluoromethyl)-1-benzothien-2-yl]heptyl}oxy)phenyl]oxy}acetate (863119-33-9) + ethyl {[2-methyl-4-({(3S)-3-[3-methyl-6-(trifluoromethyl)-1-benzothien-2-yl]heptyl}oxy)phenyl]oxy}acetate (863119-34-0)

Guidance literature:

Resolution of racemate;

upstream raw materials:

(4-hydroxy-2-methylphenoxy)acetic acid ethyl ester

2-[1-(2-bromoethyl)pentyl]-3-methyl-6-(trifluoromethyl)-1-benzothiophene

Downstream raw materials:

ethyl {[2-methyl-4-({(3R)-3-[3-methyl-6-(trifluoromethyl)-1-benzothien-2-yl]heptyl}oxy)phenyl]oxy}acetate

ethyl {[2-methyl-4-({(3S)-3-[3-methyl-6-(trifluoromethyl)-1-benzothien-2-yl]heptyl}oxy)phenyl]oxy}acetate

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