(R)-3-{3,5-dimethoxy-4-[1-methyl-2-(3,4,5-trimethoxyphenyl)ethoxyl]phenyl}-(trans)-prop-2-en-1-ol

Base Information

Chemical Name:(R)-3-{3,5-dimethoxy-4-[1-methyl-2-(3,4,5-trimethoxyphenyl)ethoxyl]phenyl}-(trans)-prop-2-en-1-ol
CAS No.:860294-70-8
Molecular Formula:C₂₃H₃₀O₇
Molecular Weight:418.487
Hs Code.:

Synonyms:(R)-3-{3,5-dimethoxy-4-[1-methyl-2-(3,4,5-trimethoxyphenyl)ethoxyl]phenyl}-(trans)-prop-2-en-1-ol

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Chemical Property of (R)-3-{3,5-dimethoxy-4-[1-methyl-2-(3,4,5-trimethoxyphenyl)ethoxyl]phenyl}-(trans)-prop-2-en-1-ol

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Technology Process of (R)-3-{3,5-dimethoxy-4-[1-methyl-2-(3,4,5-trimethoxyphenyl)ethoxyl]phenyl}-(trans)-prop-2-en-1-ol

There total 4 articles about (R)-3-{3,5-dimethoxy-4-[1-methyl-2-(3,4,5-trimethoxyphenyl)ethoxyl]phenyl}-(trans)-prop-2-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 883732-70-5
(S)-3-{3,5-dimethoxy-4-[1-methyl-2-(3,4,5-trimethoxyphenyl)ethoxyl]phenyl}-(trans)-acrylic acid ethyl ester

: 860294-70-8
(R)-3-{3,5-dimethoxy-4-[1-methyl-2-(3,4,5-trimethoxyphenyl)ethoxyl]phenyl}-(trans)-prop-2-en-1-ol

Guidance literature:: With lithium aluminium tetrahydride; aluminium trichloride; In diethyl ether; at 20 ℃; for 3h;
DOI:10.1002/jccs.200400193

Reference yield:

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 860294-70-8
(R)-3-{3,5-dimethoxy-4-[1-methyl-2-(3,4,5-trimethoxyphenyl)ethoxyl]phenyl}-(trans)-prop-2-en-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / piperidine / H₂O / 48 h / Heating

2: 45 percent / PPh₃; diisopropyl azodicarboxylate / tetrahydrofuran / 20 °C

3: 70 percent / pyridine; piperidine / 6 h / 120 °C

4: 89 percent / LiAlH₄; AlCl₃ / diethyl ether / 3 h / 20 °C

With piperidine; pyridine; lithium aluminium tetrahydride; aluminium trichloride; di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; diethyl ether; water; 2: Mitsunobu reaction;
DOI:10.1002/jccs.200400193

Reference yield:

: 134-96-3
syringic aldehyde

: 860294-70-8
(R)-3-{3,5-dimethoxy-4-[1-methyl-2-(3,4,5-trimethoxyphenyl)ethoxyl]phenyl}-(trans)-prop-2-en-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 45 percent / PPh₃; diisopropyl azodicarboxylate / tetrahydrofuran / 20 °C

2: 70 percent / pyridine; piperidine / 6 h / 120 °C

3: 89 percent / LiAlH₄; AlCl₃ / diethyl ether / 3 h / 20 °C

With piperidine; pyridine; lithium aluminium tetrahydride; aluminium trichloride; di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; diethyl ether; 1: Mitsunobu reaction;
DOI:10.1002/jccs.200400193