3-[4-(diphenylamino)piperidin-1-yl]-N-(3-methoxyphenyl)-N-methylpropanamide

Base Information

Chemical Name:3-[4-(diphenylamino)piperidin-1-yl]-N-(3-methoxyphenyl)-N-methylpropanamide
CAS No.:1610999-33-1
Molecular Formula:C₂₈H₃₃N₃O₂
Molecular Weight:443.589
Hs Code.:

Synonyms:3-[4-(diphenylamino)piperidin-1-yl]-N-(3-methoxyphenyl)-N-methylpropanamide

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Chemical Property of 3-[4-(diphenylamino)piperidin-1-yl]-N-(3-methoxyphenyl)-N-methylpropanamide

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Technology Process of 3-[4-(diphenylamino)piperidin-1-yl]-N-(3-methoxyphenyl)-N-methylpropanamide

There total 2 articles about 3-[4-(diphenylamino)piperidin-1-yl]-N-(3-methoxyphenyl)-N-methylpropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1567123-52-7
3-bromo-N-(3-methoxyphenyl)-N-methylpropanamide

: 84359-50-2
N,N-diphenylpiperidine-4-amine

: 1610999-33-1
3-[4-(diphenylamino)piperidin-1-yl]-N-(3-methoxyphenyl)-N-methylpropanamide

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1016/j.ejmech.2014.04.034

Reference yield:

: 14318-66-2
3-methoxy-N-methylaniline

: 1610999-33-1
3-[4-(diphenylamino)piperidin-1-yl]-N-(3-methoxyphenyl)-N-methylpropanamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / ethyl acetate; water / 0.33 h / 20 °C / Cooling with ice

2: triethylamine / N,N-dimethyl-formamide / 16 h / 20 °C

With sodium hydrogencarbonate; triethylamine; In water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.04.034

Reference yield: 47.0%

: 1610999-33-1
3-[4-(diphenylamino)piperidin-1-yl]-N-(3-methoxyphenyl)-N-methylpropanamide

: 1-{3-[(3-methoxyphenyl)methylamino]propyl}-N,N-diphenylpiperidin-4-amine

Guidance literature:: With diborane; In tetrahydrofuran; at 20 ℃; for 16h; Inert atmosphere; Cooling with ice;
DOI:10.1016/j.ejmech.2014.04.034