2-(benzyloxycarbonylamino)-2-(2-tert-butoxycarbonyl-1-phenylhydrazinyl)-1,3-dimethy-1,3,2-diazaphospholidin-2-ium chloride

Base Information

Chemical Name:2-(benzyloxycarbonylamino)-2-(2-tert-butoxycarbonyl-1-phenylhydrazinyl)-1,3-dimethy-1,3,2-diazaphospholidin-2-ium chloride
CAS No.:1542782-27-3
Molecular Formula:C₂₃H₃₂N₅O₄P*ClH
Molecular Weight:509.973
Hs Code.:

Synonyms:2-(benzyloxycarbonylamino)-2-(2-tert-butoxycarbonyl-1-phenylhydrazinyl)-1,3-dimethy-1,3,2-diazaphospholidin-2-ium chloride

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Chemical Property of 2-(benzyloxycarbonylamino)-2-(2-tert-butoxycarbonyl-1-phenylhydrazinyl)-1,3-dimethy-1,3,2-diazaphospholidin-2-ium chloride

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Technology Process of 2-(benzyloxycarbonylamino)-2-(2-tert-butoxycarbonyl-1-phenylhydrazinyl)-1,3-dimethy-1,3,2-diazaphospholidin-2-ium chloride

There total 1 articles about 2-(benzyloxycarbonylamino)-2-(2-tert-butoxycarbonyl-1-phenylhydrazinyl)-1,3-dimethy-1,3,2-diazaphospholidin-2-ium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 3422-03-5
benzyloxycarbonyl azide

: 6069-36-9
2-chloro-1,3-dimethyl-1,3,2-diazaphospholidine

: 42116-43-8
tert-butyl 2-phenylhydrazine-1-carboxylate

: 1542782-27-3
2-(benzyloxycarbonylamino)-2-(2-tert-butoxycarbonyl-1-phenylhydrazinyl)-1,3-dimethy-1,3,2-diazaphospholidin-2-ium chloride

Guidance literature:: 2-chloro-1,3-dimethyl-1,3,2-diazaphospholidine; tert-butyl 2-phenylhydrazine-1-carboxylate; With N-ethyl-N,N-diisopropylamine; In toluene; at 0 - 20 ℃; for 2h; Inert atmosphere;

benzyloxycarbonyl azide; In toluene; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1055/s-0033-1340058

Reference yield: 89.0%

: 1542782-27-3
2-(benzyloxycarbonylamino)-2-(2-tert-butoxycarbonyl-1-phenylhydrazinyl)-1,3-dimethy-1,3,2-diazaphospholidin-2-ium chloride

: 1542782-29-5
2-amino-2-(2-(tert-butoxycarbonyl)-1-phenylhydrazinyl)-1,3-dimethyl-1,3,2-diazaphospholidin-2-ium chloride

Guidance literature:: With triethylsilane; triethylamine; palladium dichloride; In dichloromethane; for 2h; Inert atmosphere; Reflux;
DOI:10.1055/s-0033-1340058

Reference yield:

: 1542782-27-3
2-(benzyloxycarbonylamino)-2-(2-tert-butoxycarbonyl-1-phenylhydrazinyl)-1,3-dimethy-1,3,2-diazaphospholidin-2-ium chloride

: 1542782-22-8
C₂₀H₃₁N₁₀P₃*HI

Guidance literature:: Multi-step reaction with 3 steps

1: palladium dichloride; triethylamine; triethylsilane / dichloromethane / 2 h / Inert atmosphere; Reflux

2: N-ethyl-N,N-diisopropylamine; phosphorus pentachloride / dichloromethane / 5 h / 0 - 20 °C / Inert atmosphere

3: sodium iodide; chloro-trimethyl-silane / acetonitrile / 48 h / 50 °C / Inert atmosphere

With triethylsilane; chloro-trimethyl-silane; phosphorus pentachloride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium iodide; palladium dichloride; In dichloromethane; acetonitrile;
DOI:10.1055/s-0033-1340058