<4-Chlor-phenyl>--sulfid

Base Information

Chemical Name:<4-Chlor-phenyl>--sulfid
CAS No.:93352-94-4
Molecular Formula:C₁₃H₁₁ClS
Molecular Weight:234.749
Hs Code.:

Synonyms:<4-Chlor-phenyl>--sulfid

Suppliers and Price of <4-Chlor-phenyl>--sulfid

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Chemical Property of <4-Chlor-phenyl>--sulfid

Chemical Property:

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Technology Process of <4-Chlor-phenyl>--sulfid

There total 7 articles about <4-Chlor-phenyl>--sulfid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 625-95-6
3-Iodotoluene

: 106-54-7
p-Chlorothiophenol

: 93352-94-4
<4-Chlor-phenyl>--sulfid

Guidance literature:: With caesium carbonate; 2-(diphenylphosphinyl)-benzaldoxime; copper(l) iodide; In N,N-dimethyl-formamide; at 90 ℃; for 24h;
DOI:10.1016/j.tetlet.2006.05.178

Reference yield:

: 446-34-4
2-fluoro-4-methyl-1-nitrobenzene

: 93352-94-4
<4-Chlor-phenyl>--sulfid

Guidance literature:: Multi-step reaction with 4 steps

1: Na₂CO₃

2: HCl; Sn

3: NaNO₂; HBF₄

4: H₂SO₄; Celite; Cu₂O / H₂O

With copper(I) oxide; hydrogenchloride; tin; tetrafluoroboric acid; Celite; sulfuric acid; sodium carbonate; sodium nitrite; In water; 4: Pschorr cyclization;
DOI:10.1021/ol027301t

Reference yield:

: 106-54-7
p-Chlorothiophenol

: 93352-94-4
<4-Chlor-phenyl>--sulfid

Guidance literature:: Multi-step reaction with 4 steps

1: Na₂CO₃

2: HCl; Sn

3: NaNO₂; HBF₄

4: H₂SO₄; Celite; Cu₂O / H₂O

With copper(I) oxide; hydrogenchloride; tin; tetrafluoroboric acid; Celite; sulfuric acid; sodium carbonate; sodium nitrite; In water; 4: Pschorr cyclization;
DOI:10.1021/ol027301t