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C20H26O2

Base Information
  • Chemical Name:C20H26O2
  • CAS No.:952722-06-4
  • Molecular Formula:C20H26O2
  • Molecular Weight:298.425
  • Hs Code.:
C<sub>20</sub>H<sub>26</sub>O<sub>2</sub>

Synonyms:C20H26O2

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Chemical Property of C20H26O2
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Technology Process of C20H26O2

There total 13 articles about C20H26O2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With dipyridinium dichromate; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1016/j.tetasy.2007.07.007
Guidance literature:
Multi-step reaction with 9 steps
1: Rh2(OAc)4 / CH2Cl2
2: lithium aluminium hydride / diethyl ether / 1 h / 0 °C
3: 79 percent / pyridinium chlorochromate; silica gel / CH2Cl2 / 2 h / 20 °C
4: 81 percent / lithium; liq. ammonia / 2-methyl-propan-2-ol; tetrahydrofuran / 0.17 h
5: 93 percent / sodium borohydride / methanol / 0.17 h / 0 °C
6: 89 percent / sodium hydride; tetrabutylammonium iodide / tetrahydrofuran
7: 63 percent / selenium dioxide; acetic acid / 1.5 h / Heating
8: 86 percent / lithium / tetrahydrofuran / 1 h / sonication
9: 80 percent / PDC / CH2Cl2 / 3 h / 20 °C
With sodium tetrahydroborate; lithium aluminium tetrahydride; dipyridinium dichromate; selenium(IV) oxide; ammonia; silica gel; tetra-(n-butyl)ammonium iodide; lithium; sodium hydride; acetic acid; pyridinium chlorochromate; dirhodium tetraacetate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; tert-butyl alcohol; 8: Barbier reaction;
DOI:10.1016/j.tetasy.2007.07.007
Guidance literature:
Multi-step reaction with 6 steps
1: 61 percent / Rh2(OAc)4*2H2O / CH2Cl2 / 3 h / Heating
2: 93 percent / sodium borohydride / methanol / 0.17 h / 0 °C
3: 89 percent / sodium hydride; tetrabutylammonium iodide / tetrahydrofuran
4: 63 percent / selenium dioxide; acetic acid / 1.5 h / Heating
5: 86 percent / lithium / tetrahydrofuran / 1 h / sonication
6: 80 percent / PDC / CH2Cl2 / 3 h / 20 °C
With sodium tetrahydroborate; dipyridinium dichromate; selenium(IV) oxide; tetra-(n-butyl)ammonium iodide; lithium; sodium hydride; acetic acid; dirhodium tetracetate dihydrate; In tetrahydrofuran; methanol; dichloromethane; 5: Barbier reaction;
DOI:10.1016/j.tetasy.2007.07.007
upstream raw materials:

C20H28O2

C12H18N2O

C12H20O

C13H22O

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