2-O-trans-cinnamoyl-3-O-p-methoxybenzyl-4-O-n-dodecanoyl-α-L-rhamnopyranosyl-(1→4)-2-O-2(S)-methylbutyryl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl-(1→4)-2-O-levulinoyl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate

Base Information

Chemical Name:2-O-trans-cinnamoyl-3-O-p-methoxybenzyl-4-O-n-dodecanoyl-α-L-rhamnopyranosyl-(1→4)-2-O-2(S)-methylbutyryl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl-(1→4)-2-O-levulinoyl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate
CAS No.:1448686-80-3
Molecular Formula:C₇₅H₉₈Cl₃NO₂₁
Molecular Weight:1455.96
Hs Code.:

2-O-trans-cinnamoyl-3-O-p-methoxybenzyl-4-O-n-dodecanoyl-α-L-rhamnopyranosyl-(1→4)-2-O-2(S)-methylbutyryl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl-(1→4)-2-O-levulinoyl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate

Synonyms:2-O-trans-cinnamoyl-3-O-p-methoxybenzyl-4-O-n-dodecanoyl-α-L-rhamnopyranosyl-(1→4)-2-O-2(S)-methylbutyryl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl-(1→4)-2-O-levulinoyl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate

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Chemical Property of 2-O-trans-cinnamoyl-3-O-p-methoxybenzyl-4-O-n-dodecanoyl-α-L-rhamnopyranosyl-(1→4)-2-O-2(S)-methylbutyryl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl-(1→4)-2-O-levulinoyl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate

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Technology Process of 2-O-trans-cinnamoyl-3-O-p-methoxybenzyl-4-O-n-dodecanoyl-α-L-rhamnopyranosyl-(1→4)-2-O-2(S)-methylbutyryl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl-(1→4)-2-O-levulinoyl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate

There total 1 articles about 2-O-trans-cinnamoyl-3-O-p-methoxybenzyl-4-O-n-dodecanoyl-α-L-rhamnopyranosyl-(1→4)-2-O-2(S)-methylbutyryl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl-(1→4)-2-O-levulinoyl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₇₃H₉₈O₂₁

: 545-06-2
trichloroacetonitrile

: 1448686-80-3
2-O-trans-cinnamoyl-3-O-p-methoxybenzyl-4-O-n-dodecanoyl-α-L-rhamnopyranosyl-(1→4)-2-O-2(S)-methylbutyryl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl-(1→4)-2-O-levulinoyl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 ℃; for 5h;
DOI:10.1021/ol4020255

Reference yield: 96.0%

: 1448686-76-7
C₁₁₀H₁₇₀O₂₉

: 1448686-80-3
2-O-trans-cinnamoyl-3-O-p-methoxybenzyl-4-O-n-dodecanoyl-α-L-rhamnopyranosyl-(1→4)-2-O-2(S)-methylbutyryl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl-(1→4)-2-O-levulinoyl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate

: 1448686-82-5
C₁₈₃H₂₆₆O₄₉

Guidance literature:: C₁₁₀H₁₇₀O₂₉; 2-O-trans-cinnamoyl-3-O-p-methoxybenzyl-4-O-n-dodecanoyl-α-L-rhamnopyranosyl-(1→4)-2-O-2(S)-methylbutyryl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl-(1→4)-2-O-levulinoyl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate; In dichloromethane; at 20 ℃; for 0.25h; Molecular sieve;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 - 0 ℃; for 1h; Molecular sieve;
DOI:10.1021/ol4020255