C₁₃H₁₈O₄

Base Information

• Chemical Name: C₁₃H₁₈O₄
• CAS No.: 1334334-80-3
• Molecular Formula: C₁₃H₁₈O₄
• Molecular Weight: 238.284
• Mol file: 1334334-80-3.mol

Synonyms:C₁₃H₁₈O₄

Chemical Property of C₁₃H₁₈O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₃H₁₈O₄

There total 2 articles about C₁₃H₁₈O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

C21H38O5Si (1334334-75-6) → C13H18O4 (1334334-80-3)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; for 2h; Inert atmosphere; Reflux;

DOI:10.1016/j.tetlet.2011.06.103

Reference yield:

C19H36O4Si (1334334-69-8) → C13H18O4 (1334334-80-3)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 0 - 20 °C

2: trifluoroacetic acid / dichloromethane / 2 h / Inert atmosphere; Reflux

With pyridine; trifluoroacetic acid; In dichloromethane;

DOI:10.1016/j.tetlet.2011.06.103

Reference yield: 91.0%

C13H18O4 (1334334-80-3) → (3E)-3-(cyclohexylmethylidene)oxolan-2-one (66909-46-4,66909-50-0,98441-94-2)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 0 ℃; for 0.333333h; stereospecific reaction;

DOI:10.1016/j.tetlet.2011.06.103

upstream raw materials:

C₁₉H₃₆O₄Si

C₂₁H₃₈O₅Si

Downstream raw materials:

(3E)-3-(cyclohexylmethylidene)oxolan-2-one