1,10-dicyclohexyl-1,5,10-triazadecane trihydrochloride

Base Information

Chemical Name:1,10-dicyclohexyl-1,5,10-triazadecane trihydrochloride
CAS No.:79664-23-6
Molecular Formula:C₁₉H₃₉N₃*3ClH
Molecular Weight:418.922
Hs Code.:

Synonyms:1,10-dicyclohexyl-1,5,10-triazadecane trihydrochloride

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Chemical Property of 1,10-dicyclohexyl-1,5,10-triazadecane trihydrochloride

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Technology Process of 1,10-dicyclohexyl-1,5,10-triazadecane trihydrochloride

There total 1 articles about 1,10-dicyclohexyl-1,5,10-triazadecane trihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124-20-9
N-(3-aminopropyl)-1,4-diaminobutane

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 79664-23-6
1,10-dicyclohexyl-1,5,10-triazadecane trihydrochloride

Guidance literature:: With hydrogenchloride; hydrogen; Yield given. Multistep reaction; 1) 95percent EtOH, 20 to 25 deg C, 1 to 3 atm, 72 h;
DOI:10.1021/jo00338a042

Reference yield: 98.0%

: 79664-23-6
1,10-dicyclohexyl-1,5,10-triazadecane trihydrochloride

: 7169-06-4
2,3-dimethoxybenzoyl chloride

: 79664-33-8
C₄₆H₆₃N₃O₉

Guidance literature:: With triethylamine; In tetrahydrofuran; at 60 ℃;
DOI:10.1021/jo00338a042

Reference yield:

: 79664-23-6
1,10-dicyclohexyl-1,5,10-triazadecane trihydrochloride

: 79664-32-7
N¹,N¹⁰-dicyclohexyl-N¹,N⁵,N¹⁰-tris(2,3-dihydroxybenzoyl)-1,5,10-triazadecane

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / NEt₃ / tetrahydrofuran / 60 °C

2: 60 percent / BBr₃ / CCl₄; CH₂Cl₂ / Ambient temperature

With boron tribromide; triethylamine; In tetrahydrofuran; tetrachloromethane; dichloromethane;
DOI:10.1021/jo00338a042