N-(4-cyano-2,3,5,6-tetrafluorophenyl)-1-methyl-2,3-diphenylcyclopropanecarboxamide

Base Information

Chemical Name:N-(4-cyano-2,3,5,6-tetrafluorophenyl)-1-methyl-2,3-diphenylcyclopropanecarboxamide
CAS No.:1346641-78-8
Molecular Formula:C₂₄H₁₆F₄N₂O
Molecular Weight:424.397
Hs Code.:

Synonyms:N-(4-cyano-2,3,5,6-tetrafluorophenyl)-1-methyl-2,3-diphenylcyclopropanecarboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(4-cyano-2,3,5,6-tetrafluorophenyl)-1-methyl-2,3-diphenylcyclopropanecarboxamide

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Technology Process of N-(4-cyano-2,3,5,6-tetrafluorophenyl)-1-methyl-2,3-diphenylcyclopropanecarboxamide

There total 18 articles about N-(4-cyano-2,3,5,6-tetrafluorophenyl)-1-methyl-2,3-diphenylcyclopropanecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1346640-97-8
N-(4-cyano-2,3,5,6-tetrafluorophenyl)-1-methylcyclopropanecarboxamide

: 24388-23-6
2-phenyl-4,4,5,5-tetramethyl-1,3,2-dioxoborole

: N-(4-cyano-2,3,5,6-tetrafluorophenyl)-1-methyl-2-phenylcyclopropanecarboxamide

: 1346641-78-8
N-(4-cyano-2,3,5,6-tetrafluorophenyl)-1-methyl-2,3-diphenylcyclopropanecarboxamide

Guidance literature:: With (S)-3-(2,6-difluorophenyl)-2-((((4-(trichloromethyl)heptan-4-yl)oxy)carbonyl)amino)propanoic acid; water; palladium diacetate; sodium hydrogencarbonate; silver carbonate; p-benzoquinone; In tert-Amyl alcohol; at 40 ℃; for 12h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja207607s

Reference yield: 61.0%

: 1346640-97-8
N-(4-cyano-2,3,5,6-tetrafluorophenyl)-1-methylcyclopropanecarboxamide

: 24388-23-6
2-phenyl-4,4,5,5-tetramethyl-1,3,2-dioxoborole

: N-(4-cyano-2,3,5,6-tetrafluorophenyl)-1-methyl-2-phenylcyclopropanecarboxamide

: 1346641-78-8
N-(4-cyano-2,3,5,6-tetrafluorophenyl)-1-methyl-2,3-diphenylcyclopropanecarboxamide

Guidance literature:: With water; palladium diacetate; sodium hydrogencarbonate; dimethyl sulfoxide; silver carbonate; p-benzoquinone; In tert-Amyl alcohol; at 100 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ja207607s

Reference yield:

: 1346640-97-8
N-(4-cyano-2,3,5,6-tetrafluorophenyl)-1-methylcyclopropanecarboxamide

: 24388-23-6
2-phenyl-4,4,5,5-tetramethyl-1,3,2-dioxoborole

: N-(4-cyano-2,3,5,6-tetrafluorophenyl)-1-methyl-2-phenylcyclopropanecarboxamide

: N-(4-cyano-2,3,5,6-tetrafluorophenyl)-1-methyl-2-phenylcyclopropanecarboxamide

: 1346641-78-8
N-(4-cyano-2,3,5,6-tetrafluorophenyl)-1-methyl-2,3-diphenylcyclopropanecarboxamide

Guidance literature:: With (S)-3-(2,6-difluorophenyl)-2-((((4-(trichloromethyl)heptan-4-yl)oxy)carbonyl)amino)propanoic acid; water; palladium diacetate; sodium hydrogencarbonate; silver carbonate; p-benzoquinone; In tert-Amyl alcohol; at 40 ℃; for 24h; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja207607s