CH₂OC₁₅H₁₂NCl

Base Information

• Chemical Name: CH₂OC₁₅H₁₂NCl
• CAS No.: 936840-10-7
• Molecular Formula: C₁₆H₁₄ClNO
• Molecular Weight: 271.746

Synonyms:CH₂OC₁₅H₁₂NCl

Chemical Property of CH₂OC₁₅H₁₂NCl

Chemical Property:

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Technology Process of CH₂OC₁₅H₁₂NCl

There total 2 articles about CH₂OC₁₅H₁₂NCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(4-chlorophenyl)-4-methoxybenzenemethanamine (104329-18-2) → CH2OC15H12NCl (936840-10-7)

Guidance literature:

Multi-step reaction with 3 steps

1: benzyltrimethylammonium iodine dichloride; CaCO₃ / CH₂Cl₂; methanol / 25 °C

2: CuI; diethylamine / PdCl₂(PPh₃)2 / 25 °C

3: potassium carbonate / methanol / 25 °C

With copper(l) iodide; potassium carbonate; N,N,N-trimethylbenzenemethanaminium dichloroiodate; diethylamine; calcium carbonate; bis-triphenylphosphine-palladium(II) chloride; In methanol; dichloromethane; 2: Sonogashira coupling;

DOI:10.1002/anie.200604183

Reference yield:

C11H14SiNClC8H8O → CH2OC15H12NCl (936840-10-7)

Guidance literature:

With potassium carbonate; In methanol; at 25 ℃;

DOI:10.1002/anie.200604183

Reference yield: 94.0%

CH2OC15H12NCl (936840-10-7) → C15H12ClNCH2O

Guidance literature:

With P(p-C₆H₄F)3; chloro(1,5-cyclooctadiene)rhodium(I) dimer; In N,N-dimethyl-formamide; at 85 ℃; for 2h;

DOI:10.1002/anie.200604183

upstream raw materials:

N-(4-chlorophenyl)-4-methoxybenzenemethanamine

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