[1-(3',5'-dibromobenzyl)isoquinolinium][Ni(maleonitriledithiolate)2]

Base Information

Chemical Name:[1-(3',5'-dibromobenzyl)isoquinolinium][Ni(maleonitriledithiolate)2]
CAS No.:1163300-93-3
Molecular Formula:C₈N₄NiS₄*C₁₆H₁₂Br₂N
Molecular Weight:717.155
Hs Code.:

Synonyms:[1-(3',5'-dibromobenzyl)isoquinolinium][Ni(maleonitriledithiolate)2]

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Chemical Property of [1-(3',5'-dibromobenzyl)isoquinolinium][Ni(maleonitriledithiolate)2]

Chemical Property:

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Technology Process of [1-(3',5'-dibromobenzyl)isoquinolinium][Ni(maleonitriledithiolate)2]

There total 2 articles about [1-(3',5'-dibromobenzyl)isoquinolinium][Ni(maleonitriledithiolate)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: [1-(3',5'-dibromobenzyl)isoquinolinium]2[Ni(maleonitriledithiolate)2]

: 1163300-93-3
[1-(3',5'-dibromobenzyl)isoquinolinium][Ni(maleonitriledithiolate)2]

Guidance literature:: With I₂; In acetonitrile; soln. of I2 in MeCN added to soln. of nickel complex in MeCN, mixt. stirred for 4 h; MeOH added, soln. stored overnight, crystals filtered off, washed with MeOH, dried under vac.; elem. anal.;
DOI:10.1016/j.ica.2008.11.005

Reference yield:

: 1163300-95-5
1-(3',5'-dibromobenzyl)isoquinolinium bromide

: 1163300-93-3
[1-(3',5'-dibromobenzyl)isoquinolinium][Ni(maleonitriledithiolate)2]

Guidance literature:: Multi-step reaction with 2 steps

1: water

2: I₂ / acetonitrile

With I₂; In water; acetonitrile;
DOI:10.1016/j.ica.2008.11.005