((1S,2R)-1-(4-methylphenylsulfonamido)-2,3-dihydro-1H-inden-2-yl) (2S,3S)-3-hydroxy-2-methylhexanoate

Base Information

Chemical Name:((1S,2R)-1-(4-methylphenylsulfonamido)-2,3-dihydro-1H-inden-2-yl) (2S,3S)-3-hydroxy-2-methylhexanoate
CAS No.:1147557-13-8
Molecular Formula:C₂₃H₂₉NO₅S
Molecular Weight:431.553
Hs Code.:

Synonyms:((1S,2R)-1-(4-methylphenylsulfonamido)-2,3-dihydro-1H-inden-2-yl) (2S,3S)-3-hydroxy-2-methylhexanoate

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Chemical Property of ((1S,2R)-1-(4-methylphenylsulfonamido)-2,3-dihydro-1H-inden-2-yl) (2S,3S)-3-hydroxy-2-methylhexanoate

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Technology Process of ((1S,2R)-1-(4-methylphenylsulfonamido)-2,3-dihydro-1H-inden-2-yl) (2S,3S)-3-hydroxy-2-methylhexanoate

There total 1 articles about ((1S,2R)-1-(4-methylphenylsulfonamido)-2,3-dihydro-1H-inden-2-yl) (2S,3S)-3-hydroxy-2-methylhexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 123-72-8
butyraldehyde

: 193549-82-5
(1S,2R)-1-(4-methylphenylsulfonamido)-2,3-dihydro-1H-inden-2-yl propionate

: 1147557-13-8
((1S,2R)-1-(4-methylphenylsulfonamido)-2,3-dihydro-1H-inden-2-yl) (2S,3S)-3-hydroxy-2-methylhexanoate

Guidance literature:: (1S,2R)-1-(4-methylphenylsulfonamido)-2,3-dihydro-1H-inden-2-yl propionate; With titanium tetrachloride; In dichloromethane; at 0 ℃; for 0.25h; Inert atmosphere;

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 23 ℃; Inert atmosphere;

butyraldehyde; With titanium tetrachloride; In dichloromethane; acetonitrile; at -78 ℃; for 2h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ol900412u

Reference yield: 86.0%

: 1147557-13-8
((1S,2R)-1-(4-methylphenylsulfonamido)-2,3-dihydro-1H-inden-2-yl) (2S,3S)-3-hydroxy-2-methylhexanoate

: 81927-55-1
O-benzyl 2,2,2-trichloroacetimidate

: 1147557-39-8
C₃₀H₃₅NO₅S

Guidance literature:: With trifluorormethanesulfonic acid; In dichloromethane; cyclohexane; at 0 ℃; for 6h; Inert atmosphere;
DOI:10.1021/ol900412u