1-[2-(4-benzyl-4-hydroxypiperidin-1-yl)ethyl]-3-(5-methylthieno-[3,2-b]pyridin-7-yl)urea

Base Information

Chemical Name:1-[2-(4-benzyl-4-hydroxypiperidin-1-yl)ethyl]-3-(5-methylthieno-[3,2-b]pyridin-7-yl)urea
CAS No.:1623011-20-0
Molecular Formula:C₂₃H₂₈N₄O₂S
Molecular Weight:424.567
Hs Code.:

Synonyms:1-[2-(4-benzyl-4-hydroxypiperidin-1-yl)ethyl]-3-(5-methylthieno-[3,2-b]pyridin-7-yl)urea

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Chemical Property of 1-[2-(4-benzyl-4-hydroxypiperidin-1-yl)ethyl]-3-(5-methylthieno-[3,2-b]pyridin-7-yl)urea

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Technology Process of 1-[2-(4-benzyl-4-hydroxypiperidin-1-yl)ethyl]-3-(5-methylthieno-[3,2-b]pyridin-7-yl)urea

There total 9 articles about 1-[2-(4-benzyl-4-hydroxypiperidin-1-yl)ethyl]-3-(5-methylthieno-[3,2-b]pyridin-7-yl)urea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1-(2-aminoethyl)-4-benzylpiperidin-4-ol

: C₉H₆N₂OS

: 1623011-20-0
1-[2-(4-benzyl-4-hydroxypiperidin-1-yl)ethyl]-3-(5-methylthieno-[3,2-b]pyridin-7-yl)urea

Guidance literature:: With triethylamine; In dichloromethane; for 1h;
DOI:10.1002/cmdc.201402087

Reference yield:

: 1623011-50-6
5-methylthieno[3,2-b]pyridine-7-carbonyl azide

: 1623011-20-0
1-[2-(4-benzyl-4-hydroxypiperidin-1-yl)ethyl]-3-(5-methylthieno-[3,2-b]pyridin-7-yl)urea

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 1 h / 110 °C

2: triethylamine / dichloromethane / 1 h

With triethylamine; In dichloromethane; toluene;
DOI:10.1002/cmdc.201402087

Reference yield:

: 1625612-34-1
C₉H₇NO₂S

: 1623011-20-0
1-[2-(4-benzyl-4-hydroxypiperidin-1-yl)ethyl]-3-(5-methylthieno-[3,2-b]pyridin-7-yl)urea

Guidance literature:: Multi-step reaction with 3 steps

1: diphenyl phosphoryl azide; triethylamine / N,N-dimethyl-formamide / 5 h / 20 °C

2: toluene / 1 h / 110 °C

3: triethylamine / dichloromethane / 1 h

With diphenyl phosphoryl azide; triethylamine; In dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1002/cmdc.201402087