benzyldimethylsilanyl-1-(3-furanyl)pent-1-en-3-one

Base Information

• Chemical Name: benzyldimethylsilanyl-1-(3-furanyl)pent-1-en-3-one
• CAS No.: 1104393-63-6
• Molecular Formula: C₁₈H₂₂O₂Si
• Molecular Weight: 298.457

Synonyms:benzyldimethylsilanyl-1-(3-furanyl)pent-1-en-3-one

Chemical Property of benzyldimethylsilanyl-1-(3-furanyl)pent-1-en-3-one

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Technology Process of benzyldimethylsilanyl-1-(3-furanyl)pent-1-en-3-one

There total 1 articles about benzyldimethylsilanyl-1-(3-furanyl)pent-1-en-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

1-(3-furanyl)pent-1-yn-3-one (1104393-87-4) + benzyldimethylsilane (1631-70-5) → benzyldimethylsilanyl-1-(3-furanyl)pent-1-en-3-one (1104393-63-6)

Guidance literature:

With cyclopentadienylruthenium(II) trisacetonitrile hexafluorophosphate; In acetone; at 0 - 20 ℃; for 1.67h;

DOI:10.1021/ol802289f

Reference yield: 78.0%

benzyldimethylsilanyl-1-(3-furanyl)pent-1-en-3-one (1104393-63-6) → 5-(furan-3-yl)-6-phenylhexan-3-one (1104393-92-1)

Guidance literature:

benzyldimethylsilanyl-1-(3-furanyl)pent-1-en-3-one; With tetrabutyl ammonium fluoride; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 ℃; for 0.166667h;

With dihydrogen peroxide; In tetrahydrofuran; water; N,N-dimethyl-formamide; at 80 ℃; for 14h;

DOI:10.1021/ol802289f

Reference yield: 71.0%

benzyldimethylsilanyl-1-(3-furanyl)pent-1-en-3-one (1104393-63-6) → 5-benzyl-5-ethyl-3-(furan-3-yl)-2,2-dimethyl-2,5-dihydro-1,2-oxasilole (1104393-76-1)

Guidance literature:

With lithium N-t-butyl-N-tritylamide; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 3.58333h;

DOI:10.1021/ol802289f

upstream raw materials:

1-(3-furanyl)pent-1-yn-3-one

benzyldimethylsilane

Downstream raw materials:

5-benzyl-5-ethyl-3-(furan-3-yl)-2,2-dimethyl-2,5-dihydro-1,2-oxasilole

5-(furan-3-yl)-6-phenylhexan-3-one

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