N-(4-nitrophenyl)-2-(2-furanylmethylene)hydrazinecarbothioamide

Base Information

• Chemical Name: N-(4-nitrophenyl)-2-(2-furanylmethylene)hydrazinecarbothioamide
• CAS No.: 31397-15-6
• Molecular Formula: C₁₂H₁₀N₄O₃S
• Molecular Weight: 290.302
• Mol file: 31397-15-6.mol

Synonyms:N-(4-nitrophenyl)-2-(2-furanylmethylene)hydrazinecarbothioamide

Chemical Property of N-(4-nitrophenyl)-2-(2-furanylmethylene)hydrazinecarbothioamide

Chemical Property:

Purity/Quality:

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Technology Process of N-(4-nitrophenyl)-2-(2-furanylmethylene)hydrazinecarbothioamide

There total 1 articles about N-(4-nitrophenyl)-2-(2-furanylmethylene)hydrazinecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

furfural (98-01-1) + 4-(4-nitrophenyl)-3-thiosemicarbazide (38985-70-5) → N-(4-nitrophenyl)-2-(2-furanylmethylene)hydrazinecarbothioamide (31397-15-6)

Guidance literature:

In methanol; at 20 ℃;

DOI:10.1021/acs.orglett.6b01788

Reference yield:

N-(4-nitrophenyl)-2-(2-furanylmethylene)hydrazinecarbothioamide (31397-15-6) + N-Benzylidenemethylamine (622-29-7) → C14H13N3OS

Guidance literature:

In acetonitrile; at 120 ℃; for 0.5h; Inert atmosphere; Microwave irradiation;

DOI:10.1021/acs.orglett.6b01788

upstream raw materials:

furfural

4-(4-nitrophenyl)-3-thiosemicarbazide