4-(3,4,5-trimethoxyphenyl)-5-(4-methoxy-1H-benzo[d]imidazole-7-yl) oxazole

Base Information

Chemical Name:4-(3,4,5-trimethoxyphenyl)-5-(4-methoxy-1H-benzo[d]imidazole-7-yl) oxazole
CAS No.:1403581-29-2
Molecular Formula:C₂₀H₁₉N₃O₅
Molecular Weight:381.388
Hs Code.:

Synonyms:4-(3,4,5-trimethoxyphenyl)-5-(4-methoxy-1H-benzo[d]imidazole-7-yl) oxazole

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Chemical Property of 4-(3,4,5-trimethoxyphenyl)-5-(4-methoxy-1H-benzo[d]imidazole-7-yl) oxazole

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Technology Process of 4-(3,4,5-trimethoxyphenyl)-5-(4-methoxy-1H-benzo[d]imidazole-7-yl) oxazole

There total 5 articles about 4-(3,4,5-trimethoxyphenyl)-5-(4-methoxy-1H-benzo[d]imidazole-7-yl) oxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.5%

: 1403581-61-2
4-methoxy-7-carbaldehyde-N¹-1H-benzo[d]imidazole

: 324519-54-2
5-{isocyano[(4-methylphenyl)sulfonyl]methyl}-1,2,3-trimethoxybenzene

: 1403581-29-2
4-(3,4,5-trimethoxyphenyl)-5-(4-methoxy-1H-benzo[d]imidazole-7-yl) oxazole

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃; for 25h; Reflux;
DOI:10.1016/j.ejmech.2013.08.006

Reference yield:

: 37466-89-0
3-methoxybenzene-1,2-diamine

: 1403581-29-2
4-(3,4,5-trimethoxyphenyl)-5-(4-methoxy-1H-benzo[d]imidazole-7-yl) oxazole

Guidance literature:: Multi-step reaction with 3 steps

1: 4 h / Reflux

2: trifluoroacetic acid / 36 h / Reflux

3: potassium carbonate / methanol / 25 h / 20 °C / Reflux

With potassium carbonate; trifluoroacetic acid; In methanol;
DOI:10.1016/j.ejmech.2013.08.006

Reference yield:

: 16554-45-3
2-methoxy-6-nitroaniline

: 1403581-29-2
4-(3,4,5-trimethoxyphenyl)-5-(4-methoxy-1H-benzo[d]imidazole-7-yl) oxazole

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen; palladium 10% on activated carbon / ethanol / 2 h / 20 °C

2: 4 h / Reflux

3: trifluoroacetic acid / 36 h / Reflux

4: potassium carbonate / methanol / 25 h / 20 °C / Reflux

With palladium 10% on activated carbon; hydrogen; potassium carbonate; trifluoroacetic acid; In methanol; ethanol;
DOI:10.1016/j.ejmech.2013.08.006