3-[(1,3,4-oxadiazolo-2(3H)-thion-5-yl)methylsulfanyl]-5,6-diphenyl-1,2,4-triazine

Base Information

Chemical Name:3-[(1,3,4-oxadiazolo-2(3H)-thion-5-yl)methylsulfanyl]-5,6-diphenyl-1,2,4-triazine
CAS No.:1283693-26-4
Molecular Formula:C₁₈H₁₃N₅OS₂
Molecular Weight:379.466
Hs Code.:

Synonyms:3-[(1,3,4-oxadiazolo-2(3H)-thion-5-yl)methylsulfanyl]-5,6-diphenyl-1,2,4-triazine

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Chemical Property of 3-[(1,3,4-oxadiazolo-2(3H)-thion-5-yl)methylsulfanyl]-5,6-diphenyl-1,2,4-triazine

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Technology Process of 3-[(1,3,4-oxadiazolo-2(3H)-thion-5-yl)methylsulfanyl]-5,6-diphenyl-1,2,4-triazine

There total 3 articles about 3-[(1,3,4-oxadiazolo-2(3H)-thion-5-yl)methylsulfanyl]-5,6-diphenyl-1,2,4-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 75-15-0,12122-00-8
carbon disulfide

: 95633-36-6
2-(5,6-diphenyl-1,2,4-triazin-3-ylsulphanyl)acetohydrazide

: 1283693-26-4
3-[(1,3,4-oxadiazolo-2(3H)-thion-5-yl)methylsulfanyl]-5,6-diphenyl-1,2,4-triazine

Guidance literature:: With potassium hydroxide; In ethanol; water; for 12h; Reflux;
DOI:10.1002/jhet.522

Reference yield:

: 41249-76-7
HTS 12487

: 1283693-26-4
3-[(1,3,4-oxadiazolo-2(3H)-thion-5-yl)methylsulfanyl]-5,6-diphenyl-1,2,4-triazine

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / 3 h / Reflux

2: potassium hydroxide / ethanol; water / 12 h / Reflux

With hydrazine hydrate; potassium hydroxide; In ethanol; water;
DOI:10.1002/jhet.522

Reference yield:

: 37469-24-2
5,6-diphenyl-1,2,4-triazine-3-thiol

: 1283693-26-4
3-[(1,3,4-oxadiazolo-2(3H)-thion-5-yl)methylsulfanyl]-5,6-diphenyl-1,2,4-triazine

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetone / 6 h / 20 °C

2: hydrazine hydrate / ethanol / 3 h / Reflux

3: potassium hydroxide / ethanol; water / 12 h / Reflux

With potassium carbonate; hydrazine hydrate; potassium hydroxide; In ethanol; water; acetone;
DOI:10.1002/jhet.522