Sulfuric acid (2R,3S,4R,5R,6S)-5-azido-4-benzyloxy-6-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-3-(4-methoxy-benzyloxy)-tetrahydro-pyran-2-ylmethyl ester 2,2,2-trifluoro-ethyl ester

Base Information

Chemical Name:Sulfuric acid (2R,3S,4R,5R,6S)-5-azido-4-benzyloxy-6-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-3-(4-methoxy-benzyloxy)-tetrahydro-pyran-2-ylmethyl ester 2,2,2-trifluoro-ethyl ester
CAS No.:640273-49-0
Molecular Formula:C₃₁H₄₄F₃N₃O₉SSi
Molecular Weight:719.852
Hs Code.:

Sulfuric acid (2R,3S,4R,5R,6S)-5-azido-4-benzyloxy-6-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-3-(4-methoxy-benzyloxy)-tetrahydro-pyran-2-ylmethyl ester 2,2,2-trifluoro-ethyl ester

Synonyms:Sulfuric acid (2R,3S,4R,5R,6S)-5-azido-4-benzyloxy-6-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-3-(4-methoxy-benzyloxy)-tetrahydro-pyran-2-ylmethyl ester 2,2,2-trifluoro-ethyl ester

Suppliers and Price of Sulfuric acid (2R,3S,4R,5R,6S)-5-azido-4-benzyloxy-6-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-3-(4-methoxy-benzyloxy)-tetrahydro-pyran-2-ylmethyl ester 2,2,2-trifluoro-ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Sulfuric acid (2R,3S,4R,5R,6S)-5-azido-4-benzyloxy-6-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-3-(4-methoxy-benzyloxy)-tetrahydro-pyran-2-ylmethyl ester 2,2,2-trifluoro-ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Sulfuric acid (2R,3S,4R,5R,6S)-5-azido-4-benzyloxy-6-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-3-(4-methoxy-benzyloxy)-tetrahydro-pyran-2-ylmethyl ester 2,2,2-trifluoro-ethyl ester

There total 6 articles about Sulfuric acid (2R,3S,4R,5R,6S)-5-azido-4-benzyloxy-6-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-3-(4-methoxy-benzyloxy)-tetrahydro-pyran-2-ylmethyl ester 2,2,2-trifluoro-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 371-67-5
2,2,2-trifluorodiazoethane

: Sulfuric acid mono-[(2R,3S,4R,5R,6S)-5-azido-4-benzyloxy-6-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-3-(4-methoxy-benzyloxy)-tetrahydro-pyran-2-ylmethyl] ester

: 640273-49-0
Sulfuric acid (2R,3S,4R,5R,6S)-5-azido-4-benzyloxy-6-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-3-(4-methoxy-benzyloxy)-tetrahydro-pyran-2-ylmethyl ester 2,2,2-trifluoro-ethyl ester

Guidance literature:: With citric acid; In acetonitrile; at 20 ℃;
DOI:10.1021/ol035882w

Reference yield:

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 640273-49-0
Sulfuric acid (2R,3S,4R,5R,6S)-5-azido-4-benzyloxy-6-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-3-(4-methoxy-benzyloxy)-tetrahydro-pyran-2-ylmethyl ester 2,2,2-trifluoro-ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: CSA / acetonitrile

2: NaH; n-Bu₄NI / tetrahydrofuran

3: 85 percent / Bu₂BOTf; BH₃*THF / tetrahydrofuran

4: sulfur trioxide-trimethylamine complex / dimethylformamide / 50 °C

5: citric acid / acetonitrile / 20 °C

With borane-THF; di-n-butylboryl trifluoromethanesulfonate; camphor-10-sulfonic acid; sulfur trioxide trimethylamine complex; tetra-(n-butyl)ammonium iodide; sodium hydride; citric acid; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ol035882w

Reference yield:

: 157488-88-5
thexyldimethylsilyl 2-azido-2-deoxy-β-D-glucopyranoside

: 640273-49-0
Sulfuric acid (2R,3S,4R,5R,6S)-5-azido-4-benzyloxy-6-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-3-(4-methoxy-benzyloxy)-tetrahydro-pyran-2-ylmethyl ester 2,2,2-trifluoro-ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: CSA / acetonitrile

2: NaH; n-Bu₄NI / tetrahydrofuran

3: 85 percent / Bu₂BOTf; BH₃*THF / tetrahydrofuran

4: sulfur trioxide-trimethylamine complex / dimethylformamide / 50 °C

5: citric acid / acetonitrile / 20 °C

With borane-THF; di-n-butylboryl trifluoromethanesulfonate; camphor-10-sulfonic acid; sulfur trioxide trimethylamine complex; tetra-(n-butyl)ammonium iodide; sodium hydride; citric acid; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ol035882w