N-<2-(Triphenylphosphonio)ethoxycarbonyl>threonyl-N⁶,N⁶-phthaloyllysin-chlorid

Base Information

Chemical Name:N-<2-(Triphenylphosphonio)ethoxycarbonyl>threonyl-N⁶,N⁶-phthaloyllysin-chlorid
CAS No.:86050-10-4
Molecular Formula:C₃₉H₄₁N₃O₈P*Cl
Molecular Weight:746.197
Hs Code.:

N-<2-(Triphenylphosphonio)ethoxycarbonyl>threonyl-N<sup>6</sup>,N<sup>6</sup>-phthaloyllysin-chlorid

Synonyms:N-<2-(Triphenylphosphonio)ethoxycarbonyl>threonyl-N⁶,N⁶-phthaloyllysin-chlorid

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Chemical Property of N-<2-(Triphenylphosphonio)ethoxycarbonyl>threonyl-N⁶,N⁶-phthaloyllysin-chlorid

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Technology Process of N-<2-(Triphenylphosphonio)ethoxycarbonyl>threonyl-N⁶,N⁶-phthaloyllysin-chlorid

There total 3 articles about N-<2-(Triphenylphosphonio)ethoxycarbonyl>threonyl-N⁶,N⁶-phthaloyllysin-chlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 86050-07-9
N-<2-(Triphenylphosphonio)ethoxycarbonyl>threonyl-N⁶,N⁶-phthaloyllysin-tert-butylester-chlorid

: 86050-10-4
N-<2-(Triphenylphosphonio)ethoxycarbonyl>threonyl-N⁶,N⁶-phthaloyllysin-chlorid

Guidance literature:: With hydrogenchloride; In dichloromethane; at 0 ℃; for 0.166667h;
DOI:10.1002/jlac.198319830302

Reference yield:

: 86040-70-2
Lys(Pht)-OtBu

: 86050-10-4
N-<2-(Triphenylphosphonio)ethoxycarbonyl>threonyl-N⁶,N⁶-phthaloyllysin-chlorid

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / (ethyl)-2-ethoxy-1,2-dihydro-1-quinolinecarboxylate / CH₂Cl₂ / 12 h / Ambient temperature

2: 96 percent / HCl / CH₂Cl₂ / 0.17 h / 0 °C

With hydrogenchloride; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In dichloromethane;
DOI:10.1002/jlac.198319830302

Reference yield:

: 86040-59-7
N-<2-(Triphenylphosphonio)ethoxycarbonyl>threonin-chlorid

: 86050-10-4
N-<2-(Triphenylphosphonio)ethoxycarbonyl>threonyl-N⁶,N⁶-phthaloyllysin-chlorid

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / (ethyl)-2-ethoxy-1,2-dihydro-1-quinolinecarboxylate / CH₂Cl₂ / 12 h / Ambient temperature

2: 96 percent / HCl / CH₂Cl₂ / 0.17 h / 0 °C

With hydrogenchloride; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In dichloromethane;
DOI:10.1002/jlac.198319830302