3,3'-[(1,12-dioxo-5,8-dioxa-2,11-diazadodecane-1,12-diyl)-bis(4,2-thiazolediyl)]bis-[4-hydroxybenzoic acid] dimethyl ester

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Chemical Name:3,3'-[(1,12-dioxo-5,8-dioxa-2,11-diazadodecane-1,12-diyl)-bis(4,2-thiazolediyl)]bis-[4-hydroxybenzoic acid] dimethyl ester
CAS No.:1144112-94-6
Molecular Formula:C₃₀H₃₀N₄O₁₀S₂
Molecular Weight:670.721
Hs Code.:

Synonyms:3,3'-[(1,12-dioxo-5,8-dioxa-2,11-diazadodecane-1,12-diyl)-bis(4,2-thiazolediyl)]bis-[4-hydroxybenzoic acid] dimethyl ester

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Chemical Property of 3,3'-[(1,12-dioxo-5,8-dioxa-2,11-diazadodecane-1,12-diyl)-bis(4,2-thiazolediyl)]bis-[4-hydroxybenzoic acid] dimethyl ester

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Technology Process of 3,3'-[(1,12-dioxo-5,8-dioxa-2,11-diazadodecane-1,12-diyl)-bis(4,2-thiazolediyl)]bis-[4-hydroxybenzoic acid] dimethyl ester

There total 1 articles about 3,3'-[(1,12-dioxo-5,8-dioxa-2,11-diazadodecane-1,12-diyl)-bis(4,2-thiazolediyl)]bis-[4-hydroxybenzoic acid] dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1144112-93-5
C₃₀H₃₄N₄O₁₀S₂

: 1144112-94-6
3,3'-[(1,12-dioxo-5,8-dioxa-2,11-diazadodecane-1,12-diyl)-bis(4,2-thiazolediyl)]bis-[4-hydroxybenzoic acid] dimethyl ester

Guidance literature:: With Bromotrichloromethane; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 25 ℃; for 14h; Inert atmosphere;
DOI:10.1016/j.bmc.2009.11.057

Reference yield: 96.0%

: 1144112-94-6
3,3'-[(1,12-dioxo-5,8-dioxa-2,11-diazadodecane-1,12-diyl)-bis(4,2-thiazolediyl)]bis-[4-hydroxybenzoic acid] dimethyl ester

: 1144112-95-7
3,3'-[(1,12-dithioxo-5,8-dioxa-2,11-diazadodecane-1,12-diyl)bis(4,2-thiazolediyl)]bis-[4-hydroxybenzoic acid] dimethyl ester

Guidance literature:: With Lawessons reagent; In toluene; at 110 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.bmc.2009.11.057

Reference yield: 65.0%

: 1144112-94-6
3,3'-[(1,12-dioxo-5,8-dioxa-2,11-diazadodecane-1,12-diyl)-bis(4,2-thiazolediyl)]bis-[4-hydroxybenzoic acid] dimethyl ester

: 1144112-96-8
3,3'-[(1,12-dioxo-5,8-dioxa-2,11-diazadodecane-1,12-diyl)bis(4,2-thiazolediyl)]bis-[4-hydroxybenzoic acid]

Guidance literature:: 3,3'-[(1,12-dioxo-5,8-dioxa-2,11-diazadodecane-1,12-diyl)-bis(4,2-thiazolediyl)]bis-[4-hydroxybenzoic acid] dimethyl ester; With water; sodium hydroxide; In tetrahydrofuran; at 70 ℃; for 4h; Inert atmosphere;

With hydrogenchloride; In water; at 20 ℃; pH=1; Inert atmosphere;
DOI:10.1016/j.bmc.2009.11.057