C₃₀H₄₀O₆Si

Base Information

• Chemical Name: C₃₀H₄₀O₆Si
• CAS No.: 1610594-37-0
• Molecular Formula: C₃₀H₄₀O₆Si
• Molecular Weight: 524.73
• Mol file: 1610594-37-0.mol

Synonyms:C₃₀H₄₀O₆Si

Chemical Property of C₃₀H₄₀O₆Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₄₀O₆Si

There total 11 articles about C₃₀H₄₀O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

C25H30O6 → C30H40O6Si (1610594-37-0)

Guidance literature:

With manganese(IV) oxide; In ethyl acetate; for 2h; Reflux;

DOI:10.1002/ejoc.201400028

Reference yield:

methyl 7,8-dideoxy-4-C-allyl-2,3-di-O-benzyl-4-O-methyl-L/D-glycero-α-D-galacto-oct-7-enopyranoside → C30H40O6Si (1610594-37-0)

Guidance literature:

Multi-step reaction with 2 steps

1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 1.5 h / 40 °C

2: manganese(IV) oxide / ethyl acetate / 2 h / Reflux

With manganese(IV) oxide; Hoveyda-Grubbs catalyst second generation; In dichloromethane; ethyl acetate;

DOI:10.1002/ejoc.201400028

Reference yield:

methyl 4-C-allyl-2,3-di-O-benzyl-4-O-methyl-α-D-galactopyranoside (1610594-24-5) → C30H40O6Si (1610594-37-0)

Guidance literature:

Multi-step reaction with 4 steps

1: Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C

2: tetrahydrofuran / 2 h / -78 °C

3: Hoveyda-Grubbs catalyst second generation / dichloromethane / 1.5 h / 40 °C

4: manganese(IV) oxide / ethyl acetate / 2 h / Reflux

With manganese(IV) oxide; Hoveyda-Grubbs catalyst second generation; Dess-Martin periodane; In tetrahydrofuran; dichloromethane; ethyl acetate; 2: |Grignard Reaction;

DOI:10.1002/ejoc.201400028

upstream raw materials:

methyl 4-C-allyl-2,3-di-O-benzyl-4-O-methyl-α-D-galactopyranoside

C₂₅H₃₀O₆

methyl-alpha-D-glucopyranoside

methyl 4,6-O-[(R)-(4-methoxyphenyl)methylene]-α-D-glucopyranoside