C₂₀H₂₈O₄Si

Base Information

Chemical Name:C₂₀H₂₈O₄Si
CAS No.:1334666-60-2
Molecular Formula:C₂₀H₂₈O₄Si
Molecular Weight:360.525
Hs Code.:

C<sub>20</sub>H<sub>28</sub>O<sub>4</sub>Si

Synonyms:C₂₀H₂₈O₄Si

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Chemical Property of C₂₀H₂₈O₄Si

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Technology Process of C₂₀H₂₈O₄Si

There total 6 articles about C₂₀H₂₈O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₀H₃₀O₅Si

: 90965-06-3
dimethyl 1-(1-diazo-2-oxopropyl)phosphonate

: 1334666-60-2
C₂₀H₂₈O₄Si

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃; for 8h; optical yield given as %de; Inert atmosphere;
DOI:10.1002/chem.201002930

Reference yield:

: C₂₆H₃₅NO₆Si

: 1334666-60-2
C₂₀H₂₈O₄Si

Guidance literature:: Multi-step reaction with 5 steps

1: trans-1,2-(1S,2S)-1,2-diaminocyclohexane-N,N’-bis(2’-diphenylphosphinobenzoyl); tris(dibenzylideneacetone)dipalladium(0) chloroform complex; triethylamine / dichloromethane / Inert atmosphere

2: lithium carbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.75 h / 0 °C / Inert atmosphere

3: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 21 h / 20 °C / Inert atmosphere

4: sodium periodate / tetrahydrofuran; water / 1 h / 20 °C / Inert atmosphere

5: potassium carbonate / methanol / 8 h / 20 °C / Inert atmosphere

With trans-1,2-(1S,2S)-1,2-diaminocyclohexane-N,N’-bis(2’-diphenylphosphinobenzoyl); tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; sodium periodate; osmium(VIII) oxide; lithium carbonate; potassium carbonate; 4-methylmorpholine N-oxide; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane; water; acetone;
DOI:10.1002/chem.201002930

Reference yield:

: 895153-48-7
(R)-1-((4-methoxybenzyl)oxy)-5-(trimethylsilyl)pent-4-yn-2-ol

: 1334666-60-2
C₂₀H₂₈O₄Si

Guidance literature:: Multi-step reaction with 6 steps

1: cyclopentadienylruthenium(II) trisacetonitrile hexafluorophosphate / acetone / 20 °C / Inert atmosphere

2: trans-1,2-(1S,2S)-1,2-diaminocyclohexane-N,N’-bis(2’-diphenylphosphinobenzoyl); tris(dibenzylideneacetone)dipalladium(0) chloroform complex; triethylamine / dichloromethane / Inert atmosphere

3: lithium carbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.75 h / 0 °C / Inert atmosphere

4: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 21 h / 20 °C / Inert atmosphere

5: sodium periodate / tetrahydrofuran; water / 1 h / 20 °C / Inert atmosphere

6: potassium carbonate / methanol / 8 h / 20 °C / Inert atmosphere

With trans-1,2-(1S,2S)-1,2-diaminocyclohexane-N,N’-bis(2’-diphenylphosphinobenzoyl); tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; sodium periodate; osmium(VIII) oxide; cyclopentadienylruthenium(II) trisacetonitrile hexafluorophosphate; lithium carbonate; potassium carbonate; 4-methylmorpholine N-oxide; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane; water; acetone;
DOI:10.1002/chem.201002930