O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1<*>4)-3,6-di-O-benzoyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranosyl trichloroacetimidate

Base Information

Chemical Name:O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1<*>4)-3,6-di-O-benzoyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranosyl trichloroacetimidate
CAS No.:160242-99-9
Molecular Formula:C₅₉H₄₈Cl₆N₂O₁₈
Molecular Weight:1285.75
Hs Code.:

O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1<*>4)-3,6-di-O-benzoyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranosyl trichloroacetimidate

Synonyms:O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1<*>4)-3,6-di-O-benzoyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranosyl trichloroacetimidate

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Chemical Property of O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1<*>4)-3,6-di-O-benzoyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranosyl trichloroacetimidate

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Technology Process of O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1<*>4)-3,6-di-O-benzoyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranosyl trichloroacetimidate

There total 6 articles about O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1<*>4)-3,6-di-O-benzoyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.7%

: 545-06-2
trichloroacetonitrile

: 160242-98-8
O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1<*>4)-3,6-di-O-benzoyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranose

: 160242-99-9
O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1<*>4)-3,6-di-O-benzoyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranosyl trichloroacetimidate

Guidance literature:: With potassium carbonate; In dichloromethane; for 3h; Ambient temperature;
DOI:10.1016/0008-6215(94)84179-9

Reference yield:

: 97523-60-9
benzyl O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1<*>4)-3,6-di-O-benzoyl-2-(benzoyloxyimino)-α-D-arabinohexopyranoside

: 160242-99-9
O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1<*>4)-3,6-di-O-benzoyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) BH₃, 2.) Et₃N / 1.) THF, RT, 3 h, 2.) THF, MeOH, RT, 2 h

2: 93 percent / H₂ / 10percent Pd/C / acetic acid / 24 h

3: 99.7 percent / K₂CO₃ / CH₂Cl₂ / 3 h / Ambient temperature

With borane; hydrogen; potassium carbonate; triethylamine; palladium on activated charcoal; In dichloromethane; acetic acid;
DOI:10.1016/0008-6215(94)84179-9

Reference yield:

: 160242-97-7
benzyl O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1<*>4)-3,6-di-O-benzoyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

: 160242-99-9
O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1<*>4)-3,6-di-O-benzoyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / H₂ / 10percent Pd/C / acetic acid / 24 h

2: 99.7 percent / K₂CO₃ / CH₂Cl₂ / 3 h / Ambient temperature

With hydrogen; potassium carbonate; palladium on activated charcoal; In dichloromethane; acetic acid;
DOI:10.1016/0008-6215(94)84179-9