trans-decyloxycinnamoyl chloride

Base Information

• Chemical Name: trans-decyloxycinnamoyl chloride
• CAS No.: 77251-82-2
• Molecular Formula: C₁₉H₂₇ClO₂
• Molecular Weight: 322.875
• Mol file: 77251-82-2.mol

Synonyms:trans-decyloxycinnamoyl chloride

Chemical Property of trans-decyloxycinnamoyl chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of trans-decyloxycinnamoyl chloride

There total 14 articles about trans-decyloxycinnamoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(2E)-3-[4-(decyloxy)phenyl]-2-propenoic acid (55379-98-1,1400679-03-9) → trans-decyloxycinnamoyl chloride (77251-82-2)

Guidance literature:

With thionyl chloride; In benzene; Heating;

DOI:10.1039/b403656e

Reference yield:

4-decyloxycinnamic acid (55379-98-1,1400679-03-9) → (E)-3-(4-Decyloxy-phenyl)-acryloyl chloride (77251-82-2,96288-40-3)

Guidance literature:

With thionyl chloride; N,N-dimethyl-formamide; In benzene; at 50 ℃; for 1h;

DOI:10.1021/jm00175a010

Reference yield:

para-coumaric acid (7400-08-0,50940-26-6) → (E)-3-(4-Decyloxy-phenyl)-acryloyl chloride (77251-82-2,96288-40-3)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium hydroxide / methanol / Reflux

2: thionyl chloride

With thionyl chloride; potassium hydroxide; In methanol;

DOI:10.1080/15421406.2011.591659

upstream raw materials:

(2E)-3-[4-(decyloxy)phenyl]-2-propenoic acid

1-bromo dodecane

p-Coumaric Acid

4-(decyloxy)benzaldehyde

Downstream raw materials:

(E)-3-(4-Decyloxy-phenyl)-acrylic acid 4-propoxy-phenyl ester

(E)-3-(4-Decyloxy-phenyl)-acrylic acid 4-ethoxy-phenyl ester

p-(p'-n-decyloxycinnamoyloxy) benzaldehyde

p-chlorophenyl p'-n-decyloxycinnamate