(Z)-1-(5-azido-2,5-dideoxy-β-D-erythro-pentofuranosyl)-5-(phenylmethylene)-2,4-imidazolidinedione

Base Information

Chemical Name:(Z)-1-(5-azido-2,5-dideoxy-β-D-erythro-pentofuranosyl)-5-(phenylmethylene)-2,4-imidazolidinedione
CAS No.:156270-77-8
Molecular Formula:C₁₅H₁₅N₅O₄
Molecular Weight:329.315
Hs Code.:

Synonyms:(Z)-1-(5-azido-2,5-dideoxy-β-D-erythro-pentofuranosyl)-5-(phenylmethylene)-2,4-imidazolidinedione

Suppliers and Price of (Z)-1-(5-azido-2,5-dideoxy-β-D-erythro-pentofuranosyl)-5-(phenylmethylene)-2,4-imidazolidinedione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (Z)-1-(5-azido-2,5-dideoxy-β-D-erythro-pentofuranosyl)-5-(phenylmethylene)-2,4-imidazolidinedione

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (Z)-1-(5-azido-2,5-dideoxy-β-D-erythro-pentofuranosyl)-5-(phenylmethylene)-2,4-imidazolidinedione

There total 4 articles about (Z)-1-(5-azido-2,5-dideoxy-β-D-erythro-pentofuranosyl)-5-(phenylmethylene)-2,4-imidazolidinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 156270-80-3
(Z)-1-(5-azido-2,5-dideoxy-3-O-(4-methylbenzoyl)-β-D-erythro-pentofuranosyl)-5-(phenylmethylene)-2,4-imidazolidinedione

: 156270-77-8
(Z)-1-(5-azido-2,5-dideoxy-β-D-erythro-pentofuranosyl)-5-(phenylmethylene)-2,4-imidazolidinedione

Guidance literature:: With sodium methylate; In methanol; Ambient temperature;
DOI:10.1080/15257779408013274

Reference yield:

: 170553-85-2
2′-deoxy-1′-O-methyl-5′-azido-D-ribofuranose

: 156270-77-8
(Z)-1-(5-azido-2,5-dideoxy-β-D-erythro-pentofuranosyl)-5-(phenylmethylene)-2,4-imidazolidinedione

Guidance literature:: Multi-step reaction with 3 steps

1: 40 percent / pyridine / 16 h / Ambient temperature

2: 1.) (NH₄)2SO₄, 1,1,1,3,3,3-hexamethyldisilazane, 2.) trimethylsilyl trifluoromethanesulfonate / 1.) reflux, 2.) MeCN, -50 - -30 deg C

3: 85 percent / NaOMe / methanol / Ambient temperature

With ammonium sulfate; trimethylsilyl trifluoromethanesulfonate; sodium methylate; 1,1,1,3,3,3-hexamethyl-disilazane; In pyridine; methanol;
DOI:10.1080/15257779408013274

Reference yield:

: 156270-78-9
methyl 5-azido-2,5-dideoxy-3-O-(4-methylbenzoyl)-α-D-erythro-pentofuranoside

: 156270-77-8
(Z)-1-(5-azido-2,5-dideoxy-β-D-erythro-pentofuranosyl)-5-(phenylmethylene)-2,4-imidazolidinedione

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) (NH₄)2SO₄, 1,1,1,3,3,3-hexamethyldisilazane, 2.) trimethylsilyl trifluoromethanesulfonate / 1.) reflux, 2.) MeCN, -50 - -30 deg C

2: 85 percent / NaOMe / methanol / Ambient temperature

With ammonium sulfate; trimethylsilyl trifluoromethanesulfonate; sodium methylate; 1,1,1,3,3,3-hexamethyl-disilazane; In methanol;
DOI:10.1080/15257779408013274