dimethyl (1'R,2'S,3'R,4'R)-4-butyl-4-(1',2',3',4',5'-pentabenzoxy-pentyl)-1H-pyrrole-2,5-dicarboxylate

Base Information

• Chemical Name: dimethyl (1'R,2'S,3'R,4'R)-4-butyl-4-(1',2',3',4',5'-pentabenzoxy-pentyl)-1H-pyrrole-2,5-dicarboxylate
• CAS No.: 935693-96-2
• Molecular Formula: C₅₂H₅₇NO₉
• Molecular Weight: 840.026

Synonyms:dimethyl (1'R,2'S,3'R,4'R)-4-butyl-4-(1',2',3',4',5'-pentabenzoxy-pentyl)-1H-pyrrole-2,5-dicarboxylate

Chemical Property of dimethyl (1'R,2'S,3'R,4'R)-4-butyl-4-(1',2',3',4',5'-pentabenzoxy-pentyl)-1H-pyrrole-2,5-dicarboxylate

Chemical Property:

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Technology Process of dimethyl (1'R,2'S,3'R,4'R)-4-butyl-4-(1',2',3',4',5'-pentabenzoxy-pentyl)-1H-pyrrole-2,5-dicarboxylate

There total 7 articles about dimethyl (1'R,2'S,3'R,4'R)-4-butyl-4-(1',2',3',4',5'-pentabenzoxy-pentyl)-1H-pyrrole-2,5-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

dimethyl (1'R,2'S,3'R,4'R)-5-butyl-4-(1',2',3',4',5'-pentabenzoxy-pentyl)pyridazine-3,6-dicarboxylate (935693-92-8) → dimethyl (1'R,2'S,3'R,4'R)-4-butyl-4-(1',2',3',4',5'-pentabenzoxy-pentyl)-1H-pyrrole-2,5-dicarboxylate (935693-96-2)

Guidance literature:

With acetic acid; zinc; for 0.5h; Heating;

DOI:10.1055/s-2007-968030

Reference yield: 18.0%

dimethyl (1'R,2'S,3'R,4'R)-5-butyl-4-(1',2',3',4',5'-pentabenzoxy-pentyl)pyridazine-3,6-dicarboxylate (935693-92-8) → dimethyl (1'R,2'S,3'R,4'R)-4-butyl-4-(1',2',3',4',5'-pentabenzoxy-pentyl)-1H-pyrrole-2,5-dicarboxylate (935693-96-2) + dimethyl (1'R,2'S,3'R,4'R)-4-butyl-3-(2',3',5'-tribenzoxy-1',4'-dihydroxypentyl)-1H-pyrrole-2,5-dicarboxylate

Guidance literature:

With acetic acid; zinc; for 15h; Heating;

DOI:10.1055/s-2007-968030

Reference yield: 16.0%

dimethyl (1'S,2'S,3'R,4'R)-5-butyl-4-(1',2',3',4',5'-pentabenzoxy-pentyl)pyridazine-3,6-dicarboxylate (935693-93-9) → dimethyl (1'R,2'S,3'R,4'R)-4-butyl-4-(1',2',3',4',5'-pentabenzoxy-pentyl)-1H-pyrrole-2,5-dicarboxylate (935693-96-2) + dimethyl (1'R,2'S,3'R,4'R)-4-butyl-3-(2',3',5'-tribenzoxy-1',4'-dihydroxypentyl)-1H-pyrrole-2,5-dicarboxylate

Guidance literature:

With zinc; In acetic acid; for 15h; Heating;

DOI:10.1002/ejoc.200700102

upstream raw materials:

dimethyl (1'R,2'S,3'R,4'R)-5-butyl-4-(1',2',3',4',5'-pentabenzoxy-pentyl)pyridazine-3,6-dicarboxylate

dimethyl (1'S,2'S,3'R,4'R)-5-butyl-4-(1',2',3',4',5'-pentabenzoxy-pentyl)pyridazine-3,6-dicarboxylate

(8S,9R,10R)-7,8,9,10,11-pentabenzoxyundec-5-yne

1,2,4,5-tetrazine-3,6-dicarboxylic acid dimethyl ester

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