C₃₅H₆₃NO₇Si₂

Base Information

Chemical Name:C₃₅H₆₃NO₇Si₂
CAS No.:1355616-47-5
Molecular Formula:C₃₅H₆₃NO₇Si₂
Molecular Weight:666.059
Hs Code.:

C<sub>35</sub>H<sub>63</sub>NO<sub>7</sub>Si<sub>2</sub>

Synonyms:C₃₅H₆₃NO₇Si₂

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Chemical Property of C₃₅H₆₃NO₇Si₂

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Technology Process of C₃₅H₆₃NO₇Si₂

There total 11 articles about C₃₅H₆₃NO₇Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1355616-37-3
C₂₂H₄₈O₄Si₂

: 101711-78-8,131685-53-5
(3R)-3-propionyl-4-benzyloxazolidin-2-one

: 1355616-47-5
C₃₅H₆₃NO₇Si₂

Guidance literature:: (3R)-3-propionyl-4-benzyloxazolidin-2-one; With di-n-butylboryl trifluoromethanesulfonate; triethylamine; In dichloromethane; at 0 ℃; Inert atmosphere;

C₂₂H₄₈O₄Si₂; In dichloromethane; at -78 - 0 ℃; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ml200254h

Reference yield:

: 1355616-31-7
C₁₅H₂₀O₄

: 1355616-47-5
C₃₅H₆₃NO₇Si₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

2.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 2 h / -78 °C / Inert atmosphere

2.2: 0.5 h / -78 °C / Inert atmosphere

3.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 2 h / -78 - -45 °C / Inert atmosphere

3.2: 2 h / -78 °C / Inert atmosphere

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / -45 °C / Inert atmosphere

5.1: 1H-imidazole / N,N-dimethyl-formamide / 16 h / 20 °C / Inert atmosphere

6.1: 2,6-di-tert-butyl-4-methylpyridine / dichloromethane / 48 h / 20 °C / Inert atmosphere

7.1: palladium 10% on activated carbon; hydrogen / ethanol

8.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C / Inert atmosphere

8.2: -78 - 20 °C / Inert atmosphere

9.1: di-n-butylboryl trifluoromethanesulfonate; triethylamine / dichloromethane / 0 °C / Inert atmosphere

9.2: -78 - 0 °C / Inert atmosphere

With 1H-imidazole; lithium aluminium tetrahydride; 2,6-di-tert-butyl-4-methylpyridine; oxalyl dichloride; di-n-butylboryl trifluoromethanesulfonate; palladium 10% on activated carbon; hydrogen; dimethyl sulfoxide; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; ethanol; hexane; dichloromethane; N,N-dimethyl-formamide; 8.1: Swern oxidation / 8.2: Swern oxidation;
DOI:10.1021/ml200254h

Reference yield:

: 1355616-35-1
C₂₈H₅₄O₄Si₂

: 1355616-47-5
C₃₅H₆₃NO₇Si₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: 2,6-di-tert-butyl-4-methylpyridine / dichloromethane / 48 h / 20 °C / Inert atmosphere

2.1: palladium 10% on activated carbon; hydrogen / ethanol

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C / Inert atmosphere

3.2: -78 - 20 °C / Inert atmosphere

4.1: di-n-butylboryl trifluoromethanesulfonate; triethylamine / dichloromethane / 0 °C / Inert atmosphere

4.2: -78 - 0 °C / Inert atmosphere

With 2,6-di-tert-butyl-4-methylpyridine; oxalyl dichloride; di-n-butylboryl trifluoromethanesulfonate; palladium 10% on activated carbon; hydrogen; dimethyl sulfoxide; triethylamine; In ethanol; dichloromethane; 3.1: Swern oxidation / 3.2: Swern oxidation;
DOI:10.1021/ml200254h