2-mercapto-3-phenyl-1,2,4-triazolo[1,5-a]-6,7,8,9-tetrahydro[b]thieno[2,3-d]pyrimidin-10-one

Base Information

• Chemical Name: 2-mercapto-3-phenyl-1,2,4-triazolo[1,5-a]-6,7,8,9-tetrahydro[b]thieno[2,3-d]pyrimidin-10-one
• CAS No.: 863917-84-4
• Molecular Formula: C₁₇H₁₄N₄OS₂
• Molecular Weight: 354.456

Synonyms:2-mercapto-3-phenyl-1,2,4-triazolo[1,5-a]-6,7,8,9-tetrahydro[b]thieno[2,3-d]pyrimidin-10-one

Chemical Property of 2-mercapto-3-phenyl-1,2,4-triazolo[1,5-a]-6,7,8,9-tetrahydro[b]thieno[2,3-d]pyrimidin-10-one

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-mercapto-3-phenyl-1,2,4-triazolo[1,5-a]-6,7,8,9-tetrahydro[b]thieno[2,3-d]pyrimidin-10-one

There total 5 articles about 2-mercapto-3-phenyl-1,2,4-triazolo[1,5-a]-6,7,8,9-tetrahydro[b]thieno[2,3-d]pyrimidin-10-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

C34H29N4OPS (863917-73-1) + carbon disulfide (75-15-0,12122-00-8) → 2-mercapto-3-phenyl-1,2,4-triazolo[1,5-a]-6,7,8,9-tetrahydro[b]thieno[2,3-d]pyrimidin-10-one (863917-84-4)

Guidance literature:

With triethylamine; In dichloromethane; at 40 ℃; for 18h;

DOI:10.1055/s-2005-865289

Reference yield:

phenyl isocyanate (103-71-9) → 2-mercapto-3-phenyl-1,2,4-triazolo[1,5-a]-6,7,8,9-tetrahydro[b]thieno[2,3-d]pyrimidin-10-one (863917-84-4)

Guidance literature:

Multi-step reaction with 4 steps

1: CH₂Cl₂ / 0 - 5 °C

2: 87 percent / NH₂NH₂*H₂O / ethanol / 0.17 h / 20 °C

3: 84 percent / C₂Cl₆; Et₃N / CH₂Cl₂ / 4 h / 20 °C

4: 88 percent / Et₃N / CH₂Cl₂ / 18 h / 40 °C

With hexachloroethane; hydrazine hydrate; triethylamine; In ethanol; dichloromethane; 1: aza-Wittig reaction / 4: aza-Wittig reaction;

DOI:10.1055/s-2005-865289

Reference yield:

4,5,6,7-Tetrahydro-2-(triphenylphosphoranylidenamino)benzothiophen-3-carbonsaeure-ethylester (90543-03-6) → 2-mercapto-3-phenyl-1,2,4-triazolo[1,5-a]-6,7,8,9-tetrahydro[b]thieno[2,3-d]pyrimidin-10-one (863917-84-4)

Guidance literature:

Multi-step reaction with 4 steps

1: CH₂Cl₂ / 0 - 5 °C

2: 87 percent / NH₂NH₂*H₂O / ethanol / 0.17 h / 20 °C

3: 84 percent / C₂Cl₆; Et₃N / CH₂Cl₂ / 4 h / 20 °C

4: 88 percent / Et₃N / CH₂Cl₂ / 18 h / 40 °C

With hexachloroethane; hydrazine hydrate; triethylamine; In ethanol; dichloromethane; 1: aza-Wittig reaction / 4: aza-Wittig reaction;

DOI:10.1055/s-2005-865289

upstream raw materials:

C₃₄H₂₉N₄OPS

carbon disulfide

phenyl isocyanate

4,5,6,7-Tetrahydro-2-(triphenylphosphoranylidenamino)benzothiophen-3-carbonsaeure-ethylester

Downstream raw materials:

C₁₉H₁₈N₄OS₂

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 863917-84-4 2-mercapto-3-phenyl-1,2,4-triazolo[1,5-a]-6,7,8,9-tetrahydro[b]thieno[2,3-d]pyrimidin-10-one

Send

Send

Metric Ton KG G Pound L ML

Send

Send