tert-butoxycarbonyl-L-valyl-N-(1-benzyl-3,3,3-trifluoro-2-oxopropyl)-L-prolinamide

Base Information

Chemical Name:tert-butoxycarbonyl-L-valyl-N-(1-benzyl-3,3,3-trifluoro-2-oxopropyl)-L-prolinamide
CAS No.:208593-74-2
Molecular Formula:C₂₅H₃₄F₃N₃O₅
Molecular Weight:513.557
Hs Code.:

Synonyms:tert-butoxycarbonyl-L-valyl-N-(1-benzyl-3,3,3-trifluoro-2-oxopropyl)-L-prolinamide

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Chemical Property of tert-butoxycarbonyl-L-valyl-N-(1-benzyl-3,3,3-trifluoro-2-oxopropyl)-L-prolinamide

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Technology Process of tert-butoxycarbonyl-L-valyl-N-(1-benzyl-3,3,3-trifluoro-2-oxopropyl)-L-prolinamide

There total 3 articles about tert-butoxycarbonyl-L-valyl-N-(1-benzyl-3,3,3-trifluoro-2-oxopropyl)-L-prolinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: {(S)-1-[(S)-2-(1-Benzyl-3,3,3-trifluoro-2-hydroxy-propylcarbamoyl)-pyrrolidine-1-carbonyl]-2-methyl-propyl}-carbamic acid tert-butyl ester

: 208593-74-2
tert-butoxycarbonyl-L-valyl-N-(1-benzyl-3,3,3-trifluoro-2-oxopropyl)-L-prolinamide

Guidance literature:: With Dess-Martin periodane;
DOI:10.1016/S0960-894X(98)00131-0

Reference yield:

: 124044-49-1
3-amino-1,1,1-trifluoro-4-phenyl-2-butanol

: 208593-74-2
tert-butoxycarbonyl-L-valyl-N-(1-benzyl-3,3,3-trifluoro-2-oxopropyl)-L-prolinamide

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / bis(2-oxo-3-oxazolidinyl)phosphinic chloride, Et₃N

2: 37 percent / Dess-Martin periodinane

With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; Dess-Martin periodane; triethylamine;
DOI:10.1016/S0960-894X(98)00131-0

Reference yield:

: 23361-28-6
N-(tert-butyloxycarbonyl)-L-valyl-L-proline

: 208593-74-2
tert-butoxycarbonyl-L-valyl-N-(1-benzyl-3,3,3-trifluoro-2-oxopropyl)-L-prolinamide

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / bis(2-oxo-3-oxazolidinyl)phosphinic chloride, Et₃N

2: 37 percent / Dess-Martin periodinane

With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; Dess-Martin periodane; triethylamine;
DOI:10.1016/S0960-894X(98)00131-0