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C38H60O8

Base Information
  • Chemical Name:C38H60O8
  • CAS No.:943898-15-5
  • Molecular Formula:C38H60O8
  • Molecular Weight:644.89
  • Hs Code.:
C<sub>38</sub>H<sub>60</sub>O<sub>8</sub>

Synonyms:C38H60O8

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Chemical Property of C38H60O8
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Technology Process of C38H60O8

There total 22 articles about C38H60O8 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With 2-chloro-1-methyl-pyridinium iodide; triethylamine; In acetonitrile; Heating;
DOI:10.1021/ol070517g
Guidance literature:
Multi-step reaction with 8 steps
1.1: 3.19 g / CH2Cl2 / 12 h / 20 °C
2.1: 69 percent / oxygen; copper(II) acetate monohydrate / PdCl2 / N,N-dimethyl-acetamide; H2O / 12 h / 20 °C
3.1: ethyldiisopropylamine; dibutylboron triflate / CH2Cl2; diethyl ether / -78 - -50 °C
3.2: CH2Cl2; diethyl ether / 6 h / -78 - -50 °C
3.3: 862 mg / aq. H2O2 / methanol; aq. phosphate buffer / pH 7
4.1: Et2BOMe / tetrahydrofuran; methanol / 0.25 h / -70 °C
4.2: 75 percent / NaBH4 / methanol; tetrahydrofuran / 3 h / -70 °C
5.1: 80 percent / ethyldiisopropylamine / CHCl3 / 12 h / 65 °C
6.1: 91 percent / aq. NaOH / tetrahydrofuran; methanol / 2 h / 60 °C
7.1: 86 percent / tetrabutylammonium fluoride / tetrahydrofuran / 24 h / 20 °C
8.1: 25 percent / 1-methyl-2-chloropyridinium iodide; triethylamine / acetonitrile / Heating
With sodium hydroxide; di-n-butylboryl trifluoromethanesulfonate; diethyl methoxy borane; tetrabutyl ammonium fluoride; 2-chloro-1-methyl-pyridinium iodide; oxygen; copper diacetate; triethylamine; N-ethyl-N,N-diisopropylamine; palladium dichloride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; chloroform; N,N-dimethyl acetamide; water; acetonitrile; 1.1: Wittig reaction / 2.1: Wacker reaction / 3.2: Evans aldol reaction;
DOI:10.1021/ol070517g
Guidance literature:
Multi-step reaction with 7 steps
1.1: 69 percent / oxygen; copper(II) acetate monohydrate / PdCl2 / N,N-dimethyl-acetamide; H2O / 12 h / 20 °C
2.1: ethyldiisopropylamine; dibutylboron triflate / CH2Cl2; diethyl ether / -78 - -50 °C
2.2: CH2Cl2; diethyl ether / 6 h / -78 - -50 °C
2.3: 862 mg / aq. H2O2 / methanol; aq. phosphate buffer / pH 7
3.1: Et2BOMe / tetrahydrofuran; methanol / 0.25 h / -70 °C
3.2: 75 percent / NaBH4 / methanol; tetrahydrofuran / 3 h / -70 °C
4.1: 80 percent / ethyldiisopropylamine / CHCl3 / 12 h / 65 °C
5.1: 91 percent / aq. NaOH / tetrahydrofuran; methanol / 2 h / 60 °C
6.1: 86 percent / tetrabutylammonium fluoride / tetrahydrofuran / 24 h / 20 °C
7.1: 25 percent / 1-methyl-2-chloropyridinium iodide; triethylamine / acetonitrile / Heating
With sodium hydroxide; di-n-butylboryl trifluoromethanesulfonate; diethyl methoxy borane; tetrabutyl ammonium fluoride; 2-chloro-1-methyl-pyridinium iodide; oxygen; copper diacetate; triethylamine; N-ethyl-N,N-diisopropylamine; palladium dichloride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; chloroform; N,N-dimethyl acetamide; water; acetonitrile; 1.1: Wacker reaction / 2.2: Evans aldol reaction;
DOI:10.1021/ol070517g
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