C₈H₉I₂N

Base Information

• Chemical Name: C₈H₉I₂N
• CAS No.: 1354311-18-4
• Molecular Formula: C₈H₉I₂N
• Molecular Weight: 372.975
• Mol file: 1354311-18-4.mol

Synonyms:C₈H₉I₂N

Chemical Property of C₈H₉I₂N

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₈H₉I₂N

There total 1 articles about C₈H₉I₂N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-ethyl-4-iodo-phenylamine (99471-67-7) → C8H9I2N (1354311-18-4)

Guidance literature:

With iodine; sodium hydrogencarbonate; In water; toluene; at 25 ℃; for 3h;

DOI:10.1021/acs.orglett.0c02266

Reference yield: 4.0%

C8H9I2N (1354311-18-4) + Cinnamoyl chloride (102-92-1,17082-09-6) → C17H15I2NO (1354310-97-6)

Guidance literature:

C₈H₉I₂N; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.166667h;

Cinnamoyl chloride; In tetrahydrofuran; at -78 - 20 ℃;

DOI:10.1021/ja211069f

Reference yield:

phthalic anhydride (85-44-9) + C8H9I2N (1354311-18-4) → C16H11I2NO2

Guidance literature:

With acetic acid; at 100 ℃; for 12h;

DOI:10.1021/acs.orglett.8b02538

upstream raw materials:

2-ethyl-4-iodo-phenylamine

Downstream raw materials:

C₁₇H₁₅I₂NO