Cbz-lycodine

Base Information

Chemical Name:Cbz-lycodine
CAS No.:1448802-19-4
Molecular Formula:C₂₄H₂₈N₂O₂
Molecular Weight:376.499
Hs Code.:

Synonyms:Cbz-lycodine

Suppliers and Price of Cbz-lycodine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cbz-lycodine

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of Cbz-lycodine

There total 9 articles about Cbz-lycodine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1448802-17-2
C₂₆H₃₀N₂O₂S₂

: 1448802-19-4
Cbz-lycodine

Guidance literature:: With 2,2'-azobis(isobutyronitrile); triphenylstannane; In toluene; at 110 ℃; for 0.5h;
DOI:10.1002/chem.201604647

Reference yield:

: 1448802-15-0
C₂₄H₂₆N₂O₃

: 1448802-19-4
Cbz-lycodine

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / dichloromethane / 5 h / 0 - 20 °C / Inert atmosphere

2: triphenylstannane; 2,2'-azobis(isobutyronitrile) / toluene / 0.5 h / 110 °C / Inert atmosphere

With 2,2'-azobis(isobutyronitrile); boron trifluoride diethyl etherate; triphenylstannane; In dichloromethane; toluene;
DOI:10.1002/anie.201208297

Reference yield:

: C₂₄H₂₆N₂O₃

: 1448802-19-4
Cbz-lycodine

Guidance literature:: Multi-step reaction with 3 steps

1: Daicel Chiral-Pak AS / ethanol; hexane; diethylamine / Resolution of racemate

2: boron trifluoride diethyl etherate / dichloromethane / 5 h / 0 - 20 °C / Inert atmosphere

3: triphenylstannane; 2,2'-azobis(isobutyronitrile) / toluene / 0.5 h / 110 °C / Inert atmosphere

With 2,2'-azobis(isobutyronitrile); boron trifluoride diethyl etherate; triphenylstannane; In ethanol; hexane; dichloromethane; diethylamine; toluene;
DOI:10.1002/anie.201208297