Technology Process of C15H16O3
There total 8 articles about C15H16O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
C38H39IrNOP(1+)*C32H12BF24(1-); hydrogen; triethylamine;
In
dichloromethane;
at 20 ℃;
for 10h;
under 22801.5 Torr;
enantioselective reaction;
Inert atmosphere;
Glovebox;
Autoclave;
DOI:10.1002/anie.201309521
- Guidance literature:
-
With
C36H43IrNOP(1+)*C32H12BF24(1-); hydrogen; triethylamine;
In
dichloromethane;
at 20 ℃;
for 10h;
under 22801.5 Torr;
enantioselective reaction;
Inert atmosphere;
Glovebox;
Autoclave;
DOI:10.1002/anie.201309521
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: XPhos; tris-(dibenzylideneacetone)dipalladium(0); lithium tert-butoxide / 1,4-dioxane / 0.17 h / Inert atmosphere
1.2: 5 h / 110 °C / Inert atmosphere
2.1: lithium hydroxide / tetrahydrofuran; water / 5 h / 60 °C
3.1: triethylamine; hydrogen; C38H39IrNOP(1+)*C32H12BF24(1-) / dichloromethane / 10 h / 20 °C / 22801.5 Torr / Inert atmosphere; Glovebox; Autoclave
With
tris-(dibenzylideneacetone)dipalladium(0); C38H39IrNOP(1+)*C32H12BF24(1-); hydrogen; triethylamine; lithium hydroxide; lithium tert-butoxide; XPhos;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
DOI:10.1002/anie.201309521