2-((2S,4S)-2-(4-methoxybenzyloxy)-4-(methoxymethoxy)hept-6-enyl)-1,3-dithiane

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Chemical Name:2-((2S,4S)-2-(4-methoxybenzyloxy)-4-(methoxymethoxy)hept-6-enyl)-1,3-dithiane
CAS No.:1228939-37-4
Molecular Formula:C₂₁H₃₂O₄S₂
Molecular Weight:412.615
Hs Code.:

Synonyms:2-((2S,4S)-2-(4-methoxybenzyloxy)-4-(methoxymethoxy)hept-6-enyl)-1,3-dithiane

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Chemical Property of 2-((2S,4S)-2-(4-methoxybenzyloxy)-4-(methoxymethoxy)hept-6-enyl)-1,3-dithiane

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Technology Process of 2-((2S,4S)-2-(4-methoxybenzyloxy)-4-(methoxymethoxy)hept-6-enyl)-1,3-dithiane

There total 1 articles about 2-((2S,4S)-2-(4-methoxybenzyloxy)-4-(methoxymethoxy)hept-6-enyl)-1,3-dithiane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1228939-48-7
(2S,4S)-1-(1,3-dithian-2-yl)-4-(methoxymethoxy)hept-6-en-2-ol

: 824-94-2
p-methoxybenzyl chloride

: 1228939-37-4
2-((2S,4S)-2-(4-methoxybenzyloxy)-4-(methoxymethoxy)hept-6-enyl)-1,3-dithiane

Guidance literature:: (2S,4S)-1-(1,3-dithian-2-yl)-4-(methoxymethoxy)hept-6-en-2-ol; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;

p-methoxybenzyl chloride; With tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; for 16h; Inert atmosphere; Reflux;
DOI:10.1021/jo100094d

Reference yield: 50.0%

: 1228939-34-1
(2R,4R,6R)-1-iodo-2,4,6-trimethoxyundecane

: 1228939-37-4
2-((2S,4S)-2-(4-methoxybenzyloxy)-4-(methoxymethoxy)hept-6-enyl)-1,3-dithiane

: 1228939-51-2
2-((2S,4S)-2-(4-methoxybenzyloxy)-4-(methoxymethoxy)hept-6-enyl)-2-((2R,4R,6R)-2,4,6-trimethoxyundecyl)-1,3-dithiane

Guidance literature:: 2-((2S,4S)-2-(4-methoxybenzyloxy)-4-(methoxymethoxy)hept-6-enyl)-1,3-dithiane; With n-butyllithium; sodium t-butanolate; In tetrahydrofuran; hexane; at -78 ℃; for 0.0333333h; Inert atmosphere;

(2R,4R,6R)-1-iodo-2,4,6-trimethoxyundecane; In tetrahydrofuran; hexane; for 0.166667h; Inert atmosphere;
DOI:10.1021/jo100094d