1-acetoxy-2-benzoyl-3,5-diphenylbenzene

Base Information

• Chemical Name: 1-acetoxy-2-benzoyl-3,5-diphenylbenzene
• CAS No.: 116941-57-2
• Molecular Formula: C₂₇H₂₀O₃
• Molecular Weight: 392.454
• Mol file: 116941-57-2.mol

Synonyms:1-acetoxy-2-benzoyl-3,5-diphenylbenzene

Chemical Property of 1-acetoxy-2-benzoyl-3,5-diphenylbenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-acetoxy-2-benzoyl-3,5-diphenylbenzene

There total 3 articles about 1-acetoxy-2-benzoyl-3,5-diphenylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

2,4,6-triphenylpyrilium perchlorate (1484-88-4,52991-61-4) + acetic anhydride (108-24-7) → 1,3,5-triphenylbenzene (612-71-5) + 1-acetoxy-2-benzoyl-3,5-diphenylbenzene (116941-57-2)

Guidance literature:

With potassium acetate; for 0.5h; Heating;

Reference yield:

2-Acetoxy-4,6-diphenyl-thiobenzophenon (118428-66-3) → 1-acetoxy-2-benzoyl-3,5-diphenylbenzene (116941-57-2)

Guidance literature:

With dihydrogen peroxide; In acetone; Yield given; Ambient temperature;

Reference yield:

2,4,6-triphenylthiopyrylium perchlorate (2930-37-2) → 1-acetoxy-2-benzoyl-3,5-diphenylbenzene (116941-57-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 29 percent / sodium acetate / 6 h / Heating; other condensing agents

2: 30percent H₂O₂ / acetone / Ambient temperature

With dihydrogen peroxide; sodium acetate; In acetone;

upstream raw materials:

2,4,6-triphenylpyrilium perchlorate

acetic anhydride

2-Acetoxy-4,6-diphenyl-thiobenzophenon

2,4,6-triphenylthiopyrylium perchlorate

Downstream raw materials:

2-Hydroxy-4,6-diphenyl-benzophenon