tert-butyl (2R,3R)-4-methoxycarbonyl-3-benzyloxy-1-hydroxybutan-2-ylcarbamate

Base Information

Chemical Name:tert-butyl (2R,3R)-4-methoxycarbonyl-3-benzyloxy-1-hydroxybutan-2-ylcarbamate
CAS No.:1181105-38-3
Molecular Formula:C₁₈H₂₇NO₆
Molecular Weight:353.415
Hs Code.:

Synonyms:tert-butyl (2R,3R)-4-methoxycarbonyl-3-benzyloxy-1-hydroxybutan-2-ylcarbamate

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Chemical Property of tert-butyl (2R,3R)-4-methoxycarbonyl-3-benzyloxy-1-hydroxybutan-2-ylcarbamate

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Technology Process of tert-butyl (2R,3R)-4-methoxycarbonyl-3-benzyloxy-1-hydroxybutan-2-ylcarbamate

There total 2 articles about tert-butyl (2R,3R)-4-methoxycarbonyl-3-benzyloxy-1-hydroxybutan-2-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1181105-36-1
(R)-tert-butyl 4-[(R)-2-methoxycarbonyl-1-benzyloxyethyl]-2,2-dimethyloxazolidine-3-carboxylate

: 1181105-38-3
tert-butyl (2R,3R)-4-methoxycarbonyl-3-benzyloxy-1-hydroxybutan-2-ylcarbamate

Guidance literature:: With acetic acid; In water; at 20 ℃; for 24h;
DOI:10.1016/j.tet.2009.05.054

Reference yield:

: 1181105-35-0
C₂₀H₂₉NO₆

: 1181105-38-3
tert-butyl (2R,3R)-4-methoxycarbonyl-3-benzyloxy-1-hydroxybutan-2-ylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 1 h / Reflux

2: acetic acid / water / 24 h / 20 °C

With potassium carbonate; acetic acid; In water; acetone;
DOI:10.1016/j.tet.2009.05.054

Reference yield: 98.0%

: 1181105-38-3
tert-butyl (2R,3R)-4-methoxycarbonyl-3-benzyloxy-1-hydroxybutan-2-ylcarbamate

: 142993-11-1
C₁₇H₂₅NO₆

Guidance literature:: tert-butyl (2R,3R)-4-methoxycarbonyl-3-benzyloxy-1-hydroxybutan-2-ylcarbamate; With sodium hydroxide; In methanol; water; at 20 ℃; for 3h;

With hydrogenchloride; In water;
DOI:10.1016/j.tet.2009.05.054