N,N'-di-p-toluenesulfonyl-N,N'-bis(5-O-allyl-3-deoxy-1,2-O-isopropylidene-α-D-xylofuranos-3-yl)-1,3-diaminopropane

Base Information

Chemical Name:N,N'-di-p-toluenesulfonyl-N,N'-bis(5-O-allyl-3-deoxy-1,2-O-isopropylidene-α-D-xylofuranos-3-yl)-1,3-diaminopropane
CAS No.:850165-11-6
Molecular Formula:C₃₉H₅₄N₂O₁₂S₂
Molecular Weight:806.996
Hs Code.:

Synonyms:N,N'-di-p-toluenesulfonyl-N,N'-bis(5-O-allyl-3-deoxy-1,2-O-isopropylidene-α-D-xylofuranos-3-yl)-1,3-diaminopropane

Suppliers and Price of N,N'-di-p-toluenesulfonyl-N,N'-bis(5-O-allyl-3-deoxy-1,2-O-isopropylidene-α-D-xylofuranos-3-yl)-1,3-diaminopropane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N,N'-di-p-toluenesulfonyl-N,N'-bis(5-O-allyl-3-deoxy-1,2-O-isopropylidene-α-D-xylofuranos-3-yl)-1,3-diaminopropane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N,N'-di-p-toluenesulfonyl-N,N'-bis(5-O-allyl-3-deoxy-1,2-O-isopropylidene-α-D-xylofuranos-3-yl)-1,3-diaminopropane

There total 4 articles about N,N'-di-p-toluenesulfonyl-N,N'-bis(5-O-allyl-3-deoxy-1,2-O-isopropylidene-α-D-xylofuranos-3-yl)-1,3-diaminopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 850165-10-5
C₃₃H₄₆N₂O₁₂S₂

: 106-95-6
allyl bromide

: 850165-11-6
N,N'-di-p-toluenesulfonyl-N,N'-bis(5-O-allyl-3-deoxy-1,2-O-isopropylidene-α-D-xylofuranos-3-yl)-1,3-diaminopropane

Guidance literature:: With sodium hydroxide; tetrabutylammomium bromide; In dichloromethane; water; at 25 ℃; for 12h;
DOI:10.1016/j.carres.2004.12.024

Reference yield:

: 850165-08-1
N,N'-di-p-toluenesulfonyl-N,N'-bis(3-deoxy-1,2:5,6-di-O-isopropylidene-α-D-glucofuranos-3-yl)-1,3-diaminopropane

: 850165-11-6
N,N'-di-p-toluenesulfonyl-N,N'-bis(5-O-allyl-3-deoxy-1,2-O-isopropylidene-α-D-xylofuranos-3-yl)-1,3-diaminopropane

Guidance literature:: Multi-step reaction with 3 steps

1.1: 85 percent / AcOH / H₂O / 12 h / 25 °C

2.1: NaIO₄ / methanol; H₂O / 2 h / 0 - 25 °C

2.2: 86 percent / NaBH₄ / methanol / 12 h / 25 °C

3.1: 86 percent / NaOH; Bu₄NBr / CH₂Cl₂; H₂O / 12 h / 25 °C

With sodium hydroxide; sodium periodate; tetrabutylammomium bromide; acetic acid; In methanol; dichloromethane; water;
DOI:10.1016/j.carres.2004.12.024

Reference yield:

: 850165-09-2
C₃₅H₅₀N₂O₁₄S₂

: 850165-11-6
N,N'-di-p-toluenesulfonyl-N,N'-bis(5-O-allyl-3-deoxy-1,2-O-isopropylidene-α-D-xylofuranos-3-yl)-1,3-diaminopropane

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaIO₄ / methanol; H₂O / 2 h / 0 - 25 °C

1.2: 86 percent / NaBH₄ / methanol / 12 h / 25 °C

2.1: 86 percent / NaOH; Bu₄NBr / CH₂Cl₂; H₂O / 12 h / 25 °C

With sodium hydroxide; sodium periodate; tetrabutylammomium bromide; In methanol; dichloromethane; water;
DOI:10.1016/j.carres.2004.12.024