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C39H46O12

Base Information
  • Chemical Name:C39H46O12
  • CAS No.:1051405-78-7
  • Molecular Formula:C39H46O12
  • Molecular Weight:706.787
  • Hs Code.:
C<sub>39</sub>H<sub>46</sub>O<sub>12</sub>

Synonyms:C39H46O12

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Chemical Property of C39H46O12
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Technology Process of C39H46O12

There total 14 articles about C39H46O12 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

Guidance literature:
With phenyllithium; In tetrahydrofuran; dibutyl ether; at -60 ℃; for 0.166667h; Inert atmosphere; Cooling with acetone-dry ice;
Guidance literature:
With lithium borohydride; In tetrahydrofuran; at -13 - 0 ℃; for 13.25h; ice/water/ammonium chloride bath;
Guidance literature:
Multi-step reaction with 8 steps
1.1: hydrazine / Isopropyl acetate / 1 h / 20 °C
2.1: dmap / dichloromethane / 3 h / 20 °C
3.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 22 h / 20 °C
4.1: sodium tetrahydroborate / methanol; ethanol / 5 h / 0 °C
5.1: dmap / dichloromethane / 15 h / 20 °C
5.2: 0.08 h
6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C
7.1: toluene-4-sulfonic acid / dichloromethane / 0.75 h / 20 °C
8.1: lithium borohydride / tetrahydrofuran / 13.25 h / -13 - 0 °C / ice/water/ammonium chloride bath
With dmap; sodium tetrahydroborate; lithium borohydride; tetrapropylammonium perruthennate; tetrabutyl ammonium fluoride; 4-methylmorpholine N-oxide; hydrazine; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; ethanol; dichloromethane; Isopropyl acetate;
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