4,6-O-benzylidene-2-<(R)-3-benzyloxytetradecanamido>-2-deoxy-α-D-glucopyranose 1-(dibenzyl phosphate)

Base Information

Chemical Name:4,6-O-benzylidene-2-<(R)-3-benzyloxytetradecanamido>-2-deoxy-α-D-glucopyranose 1-(dibenzyl phosphate)
CAS No.:109304-43-0
Molecular Formula:C₄₈H₆₂NO₁₀P
Molecular Weight:843.995
Hs Code.:

Synonyms:4,6-O-benzylidene-2-<(R)-3-benzyloxytetradecanamido>-2-deoxy-α-D-glucopyranose 1-(dibenzyl phosphate)

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Chemical Property of 4,6-O-benzylidene-2-<(R)-3-benzyloxytetradecanamido>-2-deoxy-α-D-glucopyranose 1-(dibenzyl phosphate)

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Technology Process of 4,6-O-benzylidene-2-<(R)-3-benzyloxytetradecanamido>-2-deoxy-α-D-glucopyranose 1-(dibenzyl phosphate)

There total 6 articles about 4,6-O-benzylidene-2-<(R)-3-benzyloxytetradecanamido>-2-deoxy-α-D-glucopyranose 1-(dibenzyl phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.7%

: 538-37-4
dibenzyl phosphochloridate

: 111789-77-6,111822-44-7
4,6-O-benzylidene-2-<(R)-3-benzyloxytetradecanamido>-2-deoxy-D-glucopyranose

: 109304-43-0
4,6-O-benzylidene-2-<(R)-3-benzyloxytetradecanamido>-2-deoxy-α-D-glucopyranose 1-(dibenzyl phosphate)

Guidance literature:: With n-butyllithium; In hexane; benzene; at -70 ℃; for 0.166667h;
DOI:10.1016/0008-6215(87)80202-1

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 109304-43-0
4,6-O-benzylidene-2-<(R)-3-benzyloxytetradecanamido>-2-deoxy-α-D-glucopyranose 1-(dibenzyl phosphate)

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-p-sulfonic acid monohydrate / dimethylformamide / 3 h / 55 - 60 °C

2: 82.7 percent / buthyl-lithium / benzene; hexane / 0.17 h / -70 °C

With n-butyllithium; toluene-4-sulfonic acid; In hexane; N,N-dimethyl-formamide; benzene;
DOI:10.1016/0008-6215(87)80202-1

Reference yield:

: 538-60-3
dibenzyl hydrogen phosphite

: 109304-43-0
4,6-O-benzylidene-2-<(R)-3-benzyloxytetradecanamido>-2-deoxy-α-D-glucopyranose 1-(dibenzyl phosphate)

Guidance literature:: Multi-step reaction with 2 steps

1: N-chlorosuccinimide / benzene / 1 h

2: 82.7 percent / buthyl-lithium / benzene; hexane / 0.17 h / -70 °C

With N-chloro-succinimide; n-butyllithium; In hexane; benzene;
DOI:10.1016/0008-6215(87)80202-1