azane;[(2R,3R,4S,5S,6R)-4,5-dihydroxy-6-(hydroxymethyl)-2-[(2R,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxyoxan-3-yl] hydrogen sulfate

Base Information

Chemical Name:azane;[(2R,3R,4S,5S,6R)-4,5-dihydroxy-6-(hydroxymethyl)-2-[(2R,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxyoxan-3-yl] hydrogen sulfate
CAS No.:91667-49-1
Molecular Formula:C₁₂H₂₂O₁₄S*H₃N
Molecular Weight:439.395
Hs Code.:
DSSTox Substance ID:DTXSID20919605
Mol file:91667-49-1.mol

azane;[(2R,3R,4S,5S,6R)-4,5-dihydroxy-6-(hydroxymethyl)-2-[(2R,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxyoxan-3-yl] hydrogen sulfate

Synonyms:2-O-sulfotrehalose;alpha,alpha-trehalose 2-sulfate;trehalose 2-sulfate

Suppliers and Price of azane;[(2R,3R,4S,5S,6R)-4,5-dihydroxy-6-(hydroxymethyl)-2-[(2R,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxyoxan-3-yl] hydrogen sulfate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 3 raw suppliers

Chemical Property of azane;[(2R,3R,4S,5S,6R)-4,5-dihydroxy-6-(hydroxymethyl)-2-[(2R,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxyoxan-3-yl] hydrogen sulfate

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
PSA：244.52000
Density:g/cm³
LogP:-4.16540
Hydrogen Bond Donor Count:9
Hydrogen Bond Acceptor Count:15
Rotatable Bond Count:6
Exact Mass:439.09957564
Heavy Atom Count:28
Complexity:579

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C(C1C(C(C(C(O1)OC2C(C(C(C(O2)CO)O)O)OS(=O)(=O)O)O)O)O)O.N
Isomeric SMILES:C([C@@H]1[C@H]([C@@H]([C@H]([C@H](O1)O[C@@H]2[C@@H]([C@H]([C@@H]([C@H](O2)CO)O)O)OS(=O)(=O)O)O)O)O)O.N

Technology Process of azane;[(2R,3R,4S,5S,6R)-4,5-dihydroxy-6-(hydroxymethyl)-2-[(2R,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxyoxan-3-yl] hydrogen sulfate

There total 3 articles about azane;[(2R,3R,4S,5S,6R)-4,5-dihydroxy-6-(hydroxymethyl)-2-[(2R,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxyoxan-3-yl] hydrogen sulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 91667-52-6
Acetic acid (2R,3R,4S,5R,6R)-3-acetoxy-2-acetoxymethyl-5-sulfooxy-6-((2R,3R,4S,5R,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-4-yl ester; compound with pyridine

: 91667-49-1
ammonium α,α-trehalose 2-sulfate

Guidance literature:: With ammonium hydroxide; In methanol;
DOI:10.1016/0008-6215(84)85355-0

Reference yield:

: 91667-48-0
ammonium 4,6:4',6'-di-O-benzylidene-α,α-trehalose 2-sulfate

: 91667-49-1
ammonium α,α-trehalose 2-sulfate

Guidance literature:: With sulfuric acid; In methanol; water; Ambient temperature;
DOI:10.1016/0008-6215(84)85355-0

Reference yield:

: 18929-82-3
4,6-O-benzylidene-α-D-glucopyranosyl-(1→1)-4',6'-O-benzylidene-α-D-glucopyranoside

: 91667-49-1
ammonium α,α-trehalose 2-sulfate

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / pyridine-sulfur trioxide / pyridine / 41 h / Ambient temperature

2: H₂SO₄ / methanol; H₂O / Ambient temperature

With sulfuric acid; sulfur trioxide pyridine complex; In pyridine; methanol; water;
DOI:10.1016/0008-6215(84)85355-0