C₁₄H₁₈O

Base Information

Chemical Name:C₁₄H₁₈O
CAS No.:1380332-23-9
Molecular Formula:C₁₄H₁₈O
Molecular Weight:202.296
Hs Code.:

Synonyms:C₁₄H₁₈O

Suppliers and Price of C₁₄H₁₈O

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₄H₁₈O

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₄H₁₈O

There total 5 articles about C₁₄H₁₈O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 1380332-22-8
C₁₄H₂₀O₂

: 1380332-24-0
C₁₄H₁₈O

: 1380332-23-9
C₁₄H₁₈O

: C₁₄H₁₈O

Guidance literature:: With toluene-4-sulfonic acid; In acetonitrile; at 25 ℃; for 30h; Inert atmosphere;
DOI:10.1021/ol301092w

Reference yield:

: 25163-50-2
4-methyl-4-pentenyl-1-tosylate

: 1380332-24-0
C₁₄H₁₈O

: 1380332-23-9
C₁₄H₁₈O

: C₁₄H₁₈O

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium iodide / acetone / 5 h / 20 °C / Inert atmosphere

2.1: tert.-butyl lithium / diethyl ether; pentane / 2.5 h / -78 °C / Inert atmosphere

2.2: 0.5 h / -78 - 20 °C / Inert atmosphere

3.1: toluene-4-sulfonic acid / acetonitrile / 30 h / 25 °C / Inert atmosphere

With tert.-butyl lithium; toluene-4-sulfonic acid; sodium iodide; In diethyl ether; acetone; acetonitrile; pentane;
DOI:10.1021/ol301092w

Reference yield:

: 22508-64-1
4-methyl-4-penten-1-ol

: 1380332-24-0
C₁₄H₁₈O

: 1380332-23-9
C₁₄H₁₈O

: C₁₄H₁₈O

Guidance literature:: Multi-step reaction with 4 steps

1.1: dmap; triethylamine / dichloromethane / 2 h / 20 °C / Inert atmosphere

2.1: sodium iodide / acetone / 5 h / 20 °C / Inert atmosphere

3.1: tert.-butyl lithium / diethyl ether; pentane / 2.5 h / -78 °C / Inert atmosphere

3.2: 0.5 h / -78 - 20 °C / Inert atmosphere

4.1: toluene-4-sulfonic acid / acetonitrile / 30 h / 25 °C / Inert atmosphere

With dmap; tert.-butyl lithium; toluene-4-sulfonic acid; triethylamine; sodium iodide; In diethyl ether; dichloromethane; acetone; acetonitrile; pentane;
DOI:10.1021/ol301092w