Technology Process of C31H56O4Si2
There total 9 articles about C31H56O4Si2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C21H44O2Si2;
With
n-butyllithium; boron trifluoride diethyl etherate;
In
tetrahydrofuran;
at -78 ℃;
(R)-benzyl glycidol;
In
tetrahydrofuran;
at -78 ℃;
Further stages.;
DOI:10.1016/j.tetlet.2007.05.021
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 80 percent / Li sand / tetrahydrofuran / 2 h / Heating
2.1: 84 percent / imidazole / CH2Cl2 / 12 h / 0 - 20 °C
3.1: n-BuLi; BF3*OEt2 / tetrahydrofuran / -78 °C
3.2: 88 percent / tetrahydrofuran / -78 °C
With
1H-imidazole; n-butyllithium; boron trifluoride diethyl etherate; lithium;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2007.05.021
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 86 percent / (n-Bu)3SnH; AIBN / benzene / 0.5 h / Heating
2.1: 83 percent / CrO3; aq. H2SO4 / acetone / 1 h / 0 - 20 °C
3.1: 82 percent / triphenylphosphine / tetrahydrofuran / 3 h / Heating
4.1: 80 percent / Li sand / tetrahydrofuran / 2 h / Heating
5.1: 84 percent / imidazole / CH2Cl2 / 12 h / 0 - 20 °C
6.1: n-BuLi; BF3*OEt2 / tetrahydrofuran / -78 °C
6.2: 88 percent / tetrahydrofuran / -78 °C
With
1H-imidazole; chromium(VI) oxide; n-butyllithium; 2,2'-azobis(isobutyronitrile); sulfuric acid; boron trifluoride diethyl etherate; tri-n-butyl-tin hydride; lithium; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; acetone; benzene;
2.1: Jones' oxidation;
DOI:10.1016/j.tetlet.2007.05.021
