5-(tert-Butyl-diphenyl-silanyloxymethyl)-isophthalic acid bis-((R)-2-benzyloxycarbonyl-1-methyl-ethyl) ester

Base Information

Chemical Name:5-(tert-Butyl-diphenyl-silanyloxymethyl)-isophthalic acid bis-((R)-2-benzyloxycarbonyl-1-methyl-ethyl) ester
CAS No.:193953-18-3
Molecular Formula:C₄₇H₅₀O₉Si
Molecular Weight:786.994
Hs Code.:

Synonyms:5-(tert-Butyl-diphenyl-silanyloxymethyl)-isophthalic acid bis-((R)-2-benzyloxycarbonyl-1-methyl-ethyl) ester

Suppliers and Price of 5-(tert-Butyl-diphenyl-silanyloxymethyl)-isophthalic acid bis-((R)-2-benzyloxycarbonyl-1-methyl-ethyl) ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-(tert-Butyl-diphenyl-silanyloxymethyl)-isophthalic acid bis-((R)-2-benzyloxycarbonyl-1-methyl-ethyl) ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-(tert-Butyl-diphenyl-silanyloxymethyl)-isophthalic acid bis-((R)-2-benzyloxycarbonyl-1-methyl-ethyl) ester

There total 5 articles about 5-(tert-Butyl-diphenyl-silanyloxymethyl)-isophthalic acid bis-((R)-2-benzyloxycarbonyl-1-methyl-ethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2672-58-4
1,3,5-tris-(methoxycarbonyl)benzene

: 193953-18-3
5-(tert-Butyl-diphenyl-silanyloxymethyl)-isophthalic acid bis-((R)-2-benzyloxycarbonyl-1-methyl-ethyl) ester

Guidance literature:: Multi-step reaction with 5 steps

1: 20.1 percent / LiAlH₄ / tetrahydrofuran / 0.17 h / 1 - 30 °C

2: 92.8 percent / DMAP / dimethylformamide / 24 h / Ambient temperature

3: 78 percent / LiOH / methanol; dioxane; H₂O / 0.5 h

4: (COCl)2 / dimethylformamide / 14 h

5: pyridine / CH₂Cl₂ / 0 deg C, 3 h, RT, 8 h

With pyridine; dmap; lithium hydroxide; lithium aluminium tetrahydride; oxalyl dichloride; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19970800402

Reference yield:

: 109862-53-5
dimethyl 5-hydroxymethylbenzene-1,3-dicarboxylate

: 193953-18-3
5-(tert-Butyl-diphenyl-silanyloxymethyl)-isophthalic acid bis-((R)-2-benzyloxycarbonyl-1-methyl-ethyl) ester

Guidance literature:: Multi-step reaction with 4 steps

1: 92.8 percent / DMAP / dimethylformamide / 24 h / Ambient temperature

2: 78 percent / LiOH / methanol; dioxane; H₂O / 0.5 h

3: (COCl)2 / dimethylformamide / 14 h

4: pyridine / CH₂Cl₂ / 0 deg C, 3 h, RT, 8 h

With pyridine; dmap; lithium hydroxide; oxalyl dichloride; In 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19970800402

Reference yield:

: 193953-06-9
5-(tert-Butyl-diphenyl-silanyloxymethyl)-isophthalic acid

: 193953-18-3
5-(tert-Butyl-diphenyl-silanyloxymethyl)-isophthalic acid bis-((R)-2-benzyloxycarbonyl-1-methyl-ethyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: (COCl)2 / dimethylformamide / 14 h

2: pyridine / CH₂Cl₂ / 0 deg C, 3 h, RT, 8 h

With pyridine; oxalyl dichloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19970800402